Technology Process of N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid
There total 1 articles about N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonia;
In
1,4-dioxane; water;
dropwise addn. of ligand in dioxane to warm (60°C) aq. soln. of rare earth salt (mixing); pptn. by aq. ammonia at pH range 6.2-7.0; 20-30 min digestion on water bath; centrifugation; washing (hot water and 20% aq. dioxane); drying at 110°C;
- Guidance literature:
-
With
ammonia;
In
1,4-dioxane; water;
dropwise addn. of ligand in dioxane to warm (60°C) aq. soln. of rare earth salt (mixing); pptn. by aq. ammonia at pH range 8.7-9.3; 20-30 min digestion on water bath; centrifugation; washing (hot water and 20% aq. dioxane); drying at 110°C;