1-TETRADECANESULFONIC ACID SODIUM SALT

Base Information

• Chemical Name: 1-TETRADECANESULFONIC ACID SODIUM SALT
• CAS No.: 6994-45-2
• Molecular Formula: C₁₄H₂₉O₃S*Na
• Molecular Weight: 300.438
• Hs Code.: 2904100000
• Mol file: 6994-45-2.mol

Synonyms:1-Tetradecanesulfonicacid, sodium salt (6CI,7CI,8CI,9CI); Sodium myristylsulfonate

Chemical Property of 1-TETRADECANESULFONIC ACID SODIUM SALT

Chemical Property:

• Melting Point: 225-227 °C
• PSA: 65.58000
• LogP: 5.31350
• Water Solubility.: almost transparency in hot Water

Purity/Quality:

98%,99%, ^*data from raw suppliers

Sodium 1-Tetradecanesulfonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Sodium Myristylsulfonate is used as a surfactant for many other reactions.

Technology Process of 1-TETRADECANESULFONIC ACID SODIUM SALT

There total 7 articles about 1-TETRADECANESULFONIC ACID SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1-Bromotetradecane (112-71-0) → sodium n-tetradecane-1-sulphonate (6994-45-2)

Guidance literature:

With tetra-n-propylammonium bromide; sodium sulfite; In water; for 20h; Time; Reflux;

Reference yield:

5-undecyl-1,2-oxathiolane 2,2-dioxide (5981-19-1) → sodium n-tetradecane-1-sulphonate (6994-45-2) + Na-Tetradec-2-ensulfonat (13513-45-6) + Na-3-Ethyl-tetradecansulfonat (82099-53-4)

Guidance literature:

With ethylaluminum dichloride; In dichloromethane; 1.) 4 h, room temperature, 2.) 1 h, 40 deg C;

Reference yield:

5-undecyl-1,2-oxathiolane 2,2-dioxide (5981-19-1) + ethylaluminum dichloride (563-43-9) → sodium n-tetradecane-1-sulphonate (6994-45-2) + Na-Tetradec-2-ensulfonat (13513-45-6) + Na-3-Ethyl-tetradecansulfonat (82099-53-4)

Guidance literature:

In dichloromethane; 1.) 4 h, room temperature, 2.) 1 h, 40 deg C;

upstream raw materials:

5-undecyl-1,2-oxathiolane 2,2-dioxide

ethylaluminum dichloride

1-Bromotetradecane

tetradecane

Downstream raw materials:

tetradecane-1-sulfonic acid

C₂₃H₄₃N₂O₂S⁽¹⁺⁾*I^(1-)

Refernces

• 1、 Fekarcha, Latifa,Tazerouti, Amel. "Surface activities, foam properties, HLB, and krafft point of some n-alkanesulfonates (C14-C18) with different isomeric distributions". . p. 419 - 431. Retrieved 2012/10/29.
• 2、 Sonnek, Georg,Mueller, Gisela. "Aluminiumalkyle mit Heteroatomen; Reaktionen von 1,3-Sultonen mit Alkylaluminiumdichloriden". . p. 102 - 103. Retrieved 2007/10/02.