1,4-Benzenedicarboxylic acid, 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl ester

Base Information

• Chemical Name: 1,4-Benzenedicarboxylic acid, 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl ester
• CAS No.: 65133-69-9
• Molecular Formula: C14H18O7
• Molecular Weight: 298.293
• Mol file: 65133-69-9.mol

Synonyms:

Chemical Property of 1,4-Benzenedicarboxylic acid, 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-Benzenedicarboxylic acid, 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl ester

There total 4 articles about 1,4-Benzenedicarboxylic acid, 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Deloxan ASP I/7 (148465-45-6) + polymethaxylylene adipamide + ethylene glycol (107-21-1) → 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl terephthalate (65133-69-9) + Bis(2-Hydroxyethyl)terephthalat (959-26-2) + diethylene glycol (111-46-6)

Guidance literature:

Deloxan ASP I/7; polymethaxylylene adipamide; at 250 ℃; under 760.051 Torr;

ethylene glycol; sodium hydroxide; at 220 ℃; under 975.098 Torr;

With cation exchange resin "AMBERLITE IR-120B"; anion exchange resin "AMBERLITE IRA₉₆SB"; cation exchange resin "AMBERLITE IR-120B"; more than 3 stages; Product distribution / selectivity;

Reference yield:

Deloxan ASP I/7 (148465-45-6) + ethylene glycol (107-21-1) → 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl terephthalate (65133-69-9) + Bis(2-Hydroxyethyl)terephthalat (959-26-2) + diethylene glycol (111-46-6)

Guidance literature:

Deloxan ASP I/7; at 280 ℃;

ethylene glycol; sodium hydroxide; at 220 ℃; Product distribution / selectivity;

Reference yield:

Deloxan ASP I/7 (148465-45-6) + ethylene glycol (107-21-1) → 2-(2-hydroxyethoxy)ethyl 2-hydroxyethyl terephthalate (65133-69-9) + Bis(2-Hydroxyethyl)terephthalat (959-26-2)

Guidance literature:

Deloxan ASP I/7; at 250 ℃; under 760.051 Torr;

ethylene glycol; sodium hydroxide; at 220 ℃; under 1125.11 Torr;

With cation exchange resin "AMBERLITE IR-120B"; anion exchange resin "AMBERLITE IRA₉₆SB"; cation exchange resin "AMBERLITE IR-120B"; more than 3 stages; Product distribution / selectivity;

upstream raw materials:

Deloxan ASP I/7

ethylene glycol

Bis(2-Hydroxyethyl)terephthalat

diethylene glycol

Refernces