(10-broModecyl)triethoxysilane

Base Information

• Chemical Name: (10-broModecyl)triethoxysilane
• CAS No.: 652159-43-8
• Molecular Formula: C16H35BrO3Si
• Molecular Weight: 383.442
• Mol file: 652159-43-8.mol

Synonyms:Silane,(10-bromodecyl)triethoxy;

Chemical Property of (10-broModecyl)triethoxysilane

Chemical Property:

• PSA: 27.69000
• LogP: 5.55050

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (10-broModecyl)triethoxysilane

There total 2 articles about (10-broModecyl)triethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 10-bromodec-1-ene (62871-09-4) → C16H35O3SiBr (652159-43-8)

Guidance literature:

10-bromodec-1-ene; With dihydrogen hexachloroplatinate; trichlorosilane; In tetrahydrofuran; Heating;

ethanol; In tetrahydrofuran; hexane; at 0 ℃; Further stages.;

DOI:10.1016/j.tet.2007.03.104

Reference yield:

9-Decen-1-ol (13019-22-2) → C16H35O3SiBr (652159-43-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: CBr₄; PPh₃ / CH₂Cl₂

2.1: hexachloroplatinic acid; trichlorosilane / tetrahydrofuran / Heating

2.2: hexane; tetrahydrofuran / 0 °C

With dihydrogen hexachloroplatinate; carbon tetrabromide; trichlorosilane; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.tet.2007.03.104

Reference yield:

C16H35O3SiBr (652159-43-8) → 10-mercaptodecyltriethoxysilane

Guidance literature:

With ammonia; thiourea; In N,N-dimethyl-formamide; at 125 ℃;

DOI:10.1016/j.tet.2007.03.104

upstream raw materials:

ethanol

10-bromodec-1-ene

9-Decen-1-ol

Refernces