DODECANEDIOIC ACID MONOETHYL ESTER

Base Information

• Chemical Name: DODECANEDIOIC ACID MONOETHYL ESTER
• CAS No.: 66003-63-2
• Molecular Formula: C14H26O4
• Molecular Weight: 258.358
• Hs Code.: 2918990090
• Mol file: 66003-63-2.mol

Synonyms:11-Ethoxycarbonyldodecanoic Acid;

Chemical Property of DODECANEDIOIC ACID MONOETHYL ESTER

Chemical Property:

• Vapor Pressure: 1.73E-06mmHg at 25°C
• Melting Point: 50oC
• Boiling Point: 184oC / 1mmHg
• Flash Point: 127.6oC
• PSA: 63.60000
• Density: 1.002g/cm3
• LogP: 3.53510
• Storage Temp.: -20°C Freezer
• Solubility.: soluble in dichloromethane

Purity/Quality:

98%,99%, ^*data from raw suppliers

11-EthoxycarbonyldodecanoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 11-Ethoxycarbonyldodecanoic Acid (cas# 66003-63-2) is a compound useful in organic synthesis.

Technology Process of DODECANEDIOIC ACID MONOETHYL ESTER

There total 10 articles about DODECANEDIOIC ACID MONOETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

12-hydroxydodecanoic acid ethyl ester (78640-13-8) → 1,12-dodecadicarboxylic acid monoethyl ester (66003-63-2)

Guidance literature:

With periodic acid; pyridinium chlorochromate; In acetonitrile; at 0 - 20 ℃; for 24h; Inert atmosphere;

Reference yield: 73.8%

diethyl dodecanedioate (10471-28-0) + 1,12-dodecanedioic acid (693-23-2) → 1,12-dodecadicarboxylic acid monoethyl ester (66003-63-2)

Guidance literature:

With sulfuric acid; In ethanol; for 4h; Heating;

Reference yield: 72.0%

diethyl dodecanedioate (10471-28-0) + ethanol (64-17-5) + 1,12-dodecanedioic acid (693-23-2) → 1,12-dodecadicarboxylic acid monoethyl ester (66003-63-2)

Guidance literature:

With sulfuric acid; for 6h; Heating;

DOI:10.1007/BF00957966

upstream raw materials:

diethyl dodecanedioate

1,12-dodecanedioic acid

ethanol

1,12-dodecanedioyl dichloride

Downstream raw materials:

monoethyl ester of dodecanedioic acid chloride

1,8-octanediyl diacetate

ethyl 15-acetoxypentadecanoate

diethyl 1,20-eicosanedicarboxylate

Refernces

• 1、 Juliá-Hernández, Francisco,Moragas, Toni,Cornella, Josep,Martin, Ruben. "Remote carboxylation of halogenated aliphatic hydrocarbons with carbon dioxide". . p. 84 - 88. Retrieved 2017/05/12.
• 2、 -. "Functionalised nanoparticles, their production and use". . . Retrieved 2014/09/03.