3-ETHYL-1-PENTANOL

Base Information

• Chemical Name: 3-ETHYL-1-PENTANOL
• CAS No.: 66225-51-2
• Molecular Formula: C7H16O
• Molecular Weight: 116.203
• Hs Code.: 2905199090
• Mol file: 66225-51-2.mol

Synonyms:1-pentanol,3-ethyl;3-ethyl-pentan-1-ol;3-Ethyl-pentanol-1;3-ETHYL-1-PENTANOL;3-ethylpentanol;3-Aethyl-pentan-1-ol;

Chemical Property of 3-ETHYL-1-PENTANOL

Chemical Property:

• Melting Point: -30.45°C (estimate)
• Refractive Index: 1.4200
• Boiling Point: 147.3°C (estimate)
• PSA: 20.23000
• Density: 0.8300
• LogP: 1.80500

Purity/Quality:

98%Min ^*data from raw suppliers

3-ethylpentan-1-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ETHYL-1-PENTANOL

There total 7 articles about 3-ETHYL-1-PENTANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

ethyl-3-ethyl-pentanoate (80246-72-6) → 3-ethyl-1-pentanol (66225-51-2)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1.5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)85889-0

Reference yield:

ethyl 3-ethylpent-2-enoate (15249-93-1) → 3-ethyl-1-pentanol (66225-51-2)

Guidance literature:

ethyl 3-ethylpent-2-enoate; With hydrogen; palladium 10% on activated carbon; In methanol; at 25 ℃; for 12h; under 760.051 Torr;

With lithium aluminium tetrahydride; In tetrahydrofuran; methanol; Product distribution / selectivity;

Reference yield:

pentan-3-one (96-22-0) → 3-ethyl-1-pentanol (66225-51-2)

Guidance literature:

Multi-step reaction with 2 steps

2: 89 percent / lithium aluminium hydride / diethyl ether / 1.5 h / Ambient temperature

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1016/S0040-4020(01)85889-0

upstream raw materials:

(E)-3-ethylpent-3-en-1-ol

formaldehyd

2-ethyl-1-bromobutane

ethyl-3-ethyl-pentanoate

Downstream raw materials:

(S)-2-(1,2-dibenzyloxycarbonylhydrazinyl)-3-ethylpentan-1-ol

3-Ethyl-valeramid

3-ethylpentane

3-ethylpentanoic acid

Refernces

• 1、 -. "Process for the Preparation of Beta-Amino Alcohol". . . Retrieved 2013/02/28.
• 2、 Belavoine, Gilbert,Barton, Derek H. R.,Boivin, Jean,Gref, Aurore,Coupanec, Pascale Le,et al.. "FUNCTIONALISATION OF SATURATED HYDROCARBONS. Part X. A COMPARATIVE STUDY OF CHEMICAL AND ELECTROCHEMICAL PROCESSES (GIF AND GIF-ORSAY SYSTEMS) IN PYRIDINE, IN ACETONE AND IN PYRIDINE-CO-SOLVENT MIXTURES". . p. 1091 - 1106. Retrieved 2007/10/02.