Technology Process of Benzoic acid, 5-[[4-(dimethylamino)phenyl]azo]-2-nitro-,
11-carboxy-1-hexylundecyl ester
There total 4 articles about Benzoic acid, 5-[[4-(dimethylamino)phenyl]azo]-2-nitro-,
11-carboxy-1-hexylundecyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) red phosphorus, iodine, 2.) conc. HCl / 1.) carbon disulfide, 40 deg C, 4 h, 2.) ethyl alcohol, 24 h, reflux
2: 1.) sodium acetate, silver nitrate, 3.) dry hydrogen chloride / 1.) ethanol, water, 2.) anhydr. benzene, 30 deg C, 30 h
With
hydrogenchloride; phosphorus; iodine; sodium acetate; silver nitrate;
DOI:10.1021/ja00527a004
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) conc. HCL, acetic acid, pentyl nitrite, 2.) aq. sodium acetate / 1.) 6 deg C, 2.) 2 h, pH 2.5
2: 1.) sodium acetate, silver nitrate, 3.) dry hydrogen chloride / 1.) ethanol, water, 2.) anhydr. benzene, 30 deg C, 30 h
With
hydrogenchloride; n-Amyl nitrite; sodium acetate; silver nitrate; acetic acid;
DOI:10.1021/ja00527a004
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) conc. HCL, acetic acid, pentyl nitrite, 2.) aq. sodium acetate / 1.) 6 deg C, 2.) 2 h, pH 2.5
2: 1.) sodium acetate, silver nitrate, 3.) dry hydrogen chloride / 1.) ethanol, water, 2.) anhydr. benzene, 30 deg C, 30 h
With
hydrogenchloride; n-Amyl nitrite; sodium acetate; silver nitrate; acetic acid;
DOI:10.1021/ja00527a004
