Amidosulfenyl chloride, dibutyl-

Base Information

• Chemical Name: Amidosulfenyl chloride, dibutyl-
• CAS No.: 6541-82-8
• Molecular Formula: C8H18 Cl N S
• Molecular Weight: 195.757
• Hs Code.: 2930909090
• DSSTox Substance ID: DTXSID1064409
• Nikkaji Number: J421.822A
• Wikidata: Q81991528
• Mol file: 6541-82-8.mol

Synonyms:6541-82-8;Amidosulfenyl chloride, dibutyl-;Di-N-butyl Amidosulfenyl Chloride;(dibutylamino) thiohypochlorite;Dibutyl amidosulfenyl chloride;Amidosulfenyl chloride, N,N-dibutyl-;(Chlorothio)dibutylamine;C8H18ClNS;dibutylaminosulfenylchloride;dibutylaminosulfenyl chloride;C8-H18-Cl-N-S;SCHEMBL3961622;DTXSID1064409;N,N-di-n-butylaminosulfenyl chloride;FT-0666526

Chemical Property of Amidosulfenyl chloride, dibutyl-

Chemical Property:

• Vapor Pressure: 0.0413mmHg at 25°C
• Boiling Point: 238.9oC at 760 mmHg
• PKA: -0.16±0.70(Predicted)
• Flash Point: 98.3oC
• PSA: 42.04000
• Density: 1.013g/cm3
• LogP: 4.11240
• Solubility.: Chloroform, Dichloromethane, Ethyl Acetate, Hexane, Methanol
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 195.0848484
• Heavy Atom Count: 11
• Complexity: 72.5

Purity/Quality:

99% ^*data from raw suppliers

Di-N-butylAmidosulfenylChloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCN(CCCC)SCl
• Uses: reagent used in the preparation of pesticides DIBUTYL AMIDOSULFENYL CHLORIDE used in the preparation of pesticides

Technology Process of Amidosulfenyl chloride, dibutyl-

There total 5 articles about Amidosulfenyl chloride, dibutyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-bis-(dibutylamino)disulfide (67271-09-4) → N,N-di-n-butylaminosulfenyl chloride (6541-82-8)

Guidance literature:

With sulfuryl dichloride;

DOI:10.1021/jo00414a033

Reference yield:

dibutylamine (111-92-2) → N,N-di-n-butylaminosulfenyl chloride (6541-82-8)

Guidance literature:

With sulfur dichloride;

Reference yield:

sulphur dichloride + dibutylamine (111-92-2) → N,N-di-n-butylaminosulfenyl chloride (6541-82-8)

Guidance literature:

In tetrachloromethane; hexane;

upstream raw materials:

dibutylamine

N,N'-bis-(dibutylamino)disulfide

Downstream raw materials:

carbosulfan

Refernces

• 1、 Wang, Qingmin,Cheng, Junran,Huang, Runqin. "Synthesis and insecticidal evaluation of novel N-(S-amino)sulfenylated derivatives of diacylhydrazines". . p. 1250 - 1253. Retrieved 2007/10/03.
• 2、 Hatch III. "Synthesis of N,N-dialkylaminosulfenylcarbamate insecticides via carbamoyl fluorides". . p. 3953 - 3957. Retrieved 2007/10/09.