Benzoic acid, 3-nitro-, silver(1+) salt

Base Information

• Chemical Name: Benzoic acid, 3-nitro-, silver(1+) salt
• CAS No.: 72254-96-7
• Molecular Formula: C7H5NO4.Ag
• Molecular Weight: 273.981
• Mol file: 72254-96-7.mol

Synonyms:

Chemical Property of Benzoic acid, 3-nitro-, silver(1+) salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3-nitro-, silver(1+) salt

There total 1 articles about Benzoic acid, 3-nitro-, silver(1+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

silver(l) oxide (20667-12-3) + 3-nitrobenzoic acid (121-92-6) → Silber-(3-nitro-benzoat) (72254-96-7)

Guidance literature:

In acetonitrile; at 20 ℃; for 2h; Darkness;

DOI:10.1021/jacs.7b13305

Reference yield:

Silber-(3-nitro-benzoat) (72254-96-7) → m-nitrobromobenzene (585-79-5)

Guidance literature:

With tetrachloromethane; bromine;

DOI:10.1021/ja01163a105 DOI:10.1021/ja01163a106

Reference yield:

Silber-(3-nitro-benzoat) (72254-96-7) → nitrobenzene (98-95-3,26969-40-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / Darkness

2: water / d₇-N,N-dimethylformamide / 2.5 h / 100 °C / Inert atmosphere; Glovebox; Sealed tube; Darkness

With water; In d₇-N,N-dimethylformamide; acetonitrile;

DOI:10.1021/jacs.7b13305

upstream raw materials:

silver(l) oxide

3-nitrobenzoic acid

Downstream raw materials:

m-nitrobromobenzene

1,2-Ethylen-bis-(m-nitrobenzoat)

1,2,3-tris-(3-nitro-benzoyloxy)-propane

nitrobenzene

Refernces