7,8,9,10-Tetrachloro-6B,10A-dihydrofluoranthene

Base Information

• Chemical Name: 7,8,9,10-Tetrachloro-6B,10A-dihydrofluoranthene
• CAS No.: 72541-91-4
• Molecular Formula: C16H8Cl4
• DSSTox Substance ID: DTXSID90503550
• Mol file: 72541-91-4.mol

Synonyms:72541-91-4;7,8,9,10-TETRACHLORO-6B,10A-DIHYDROFLUORANTHENE;DTXSID90503550

Chemical Property of 7,8,9,10-Tetrachloro-6B,10A-dihydrofluoranthene

Chemical Property:

• XLogP3: 5.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 341.935061
• Heavy Atom Count: 20
• Complexity: 463

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC2=C3C(=C1)C4C(C3=CC=C2)C(=C(C(=C4Cl)Cl)Cl)Cl

Technology Process of 7,8,9,10-Tetrachloro-6B,10A-dihydrofluoranthene

There total 3 articles about 7,8,9,10-Tetrachloro-6B,10A-dihydrofluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-ethoxycarbonyl-(2,3,4,5-tetrachloro-1-thiophenio)amide (90454-50-5) + buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → 7,8,9,10-Tetrachloro-6b,10a-dihydro-fluoranthene (72541-91-4) + 3,6-Dihydro-[1,2]thiazine-2-carboxylic acid ethyl ester (95308-71-7)

Guidance literature:

With acenaphthylene; In chloroform; at 20 ℃; for 1h; Yield given. Yields of byproduct given;

DOI:10.1039/c39840001144

Reference yield:

N-ethoxycarbonyl-(2,3,4,5-tetrachloro-1-thiophenio)amide (90454-50-5) + acenaphthylene (208-96-8,25036-01-5) → 7,8,9,10-Tetrachloro-6b,10a-dihydro-fluoranthene (72541-91-4) + 3,6-Dihydro-[1,2]thiazine-2-carboxylic acid ethyl ester (95308-71-7)

Guidance literature:

With buta-1,3-diene; In chloroform; at 20 ℃; for 1h; Yield given. Yields of byproduct given;

DOI:10.1039/c39840001144

Reference yield:

N-ethoxycarbonyl-(2,3,4,5-tetrachloro-1-thiophenio)amide (90454-50-5) + cyclohexene (110-83-8) → 7,8,9,10-Tetrachloro-6b,10a-dihydro-fluoranthene (72541-91-4) + C9H15NO2S (95308-72-8)

Guidance literature:

With acenaphthylene; at 20 ℃; for 1h; Yield given. Yields of byproduct given;

DOI:10.1039/c39840001144

upstream raw materials:

N-ethoxycarbonyl-(2,3,4,5-tetrachloro-1-thiophenio)amide

buta-1,3-diene

acenaphthylene

cyclohexene

Refernces