Acenaphthylene, octachloro-

Base Information

• Chemical Name: Acenaphthylene, octachloro-
• CAS No.: 7267-16-5
• Molecular Formula: C12Cl8
• Molecular Weight: 427.756
• Mol file: 7267-16-5.mol

Synonyms:Perchloracenaphthylen;perchloroacenaphthylene;Acenaphthylene,octachloro;octachloroacenaphthylene;

Chemical Property of Acenaphthylene, octachloro-

Chemical Property:

• Melting Point: 375 °C
• Boiling Point: 505.9±50.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.94±0.1 g/cm3(Predicted)
• LogP: 8.37700

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acenaphthylene, octachloro-

There total 5 articles about Acenaphthylene, octachloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

→ hexachlorobenzene (118-74-1,67471-27-6) + octachloroacenaphthylene (7267-16-5) + decachlorocorannulene (191352-26-8)

Guidance literature:

With chlorine; In toluene; under 105.008 Torr;

Reference yield:

tetrachloromethane (56-23-5) → octachloronaphthalene (2234-13-1) + hexachlorobenzene (118-74-1,67471-27-6) + octachloroacenaphthylene (7267-16-5) + decachlorocorannulene (191352-26-8)

Guidance literature:

Further byproducts given; Electrochemical reaction; arc discharge; copper electrodes (gap 1 mm); arc voltage was 10 kV in 20 kHz; arc current was 20-50 mA;

DOI:10.1021/ja970238w

Reference yield:

chloroform (67-66-3,8013-54-5) → octachloronaphthalene (2234-13-1) + hexachlorobenzene (118-74-1,67471-27-6) + octachloroacenaphthylene (7267-16-5) + decachlorocorannulene (191352-26-8)

Guidance literature:

for 5h; Further byproducts given; Electrochemical reaction; arc discharge; copper electrodes (gap 1 mm); arc voltage was 10 kV in 20 kHz; arc current was 20-50 mA;

DOI:10.1021/ja970238w

upstream raw materials:

tetrachloromethane

chloroform

Decachlorobiphenyl

Downstream raw materials:

4,7-dichloro-1,2,3,5,6,8-hexakis(4-methoxy-phenylsulfanyl)acenaphthylene

Refernces

• 1、 Bleise,Kleist,Guenther,Schwuger. "Formation of octachloroacenaphthylene in the pyrolysis of decachlorobiphenyl". . p. 655 - 666. Retrieved 2007/10/03.