Technology Process of Benzenecarboximidoyl chloride, N-hydroxy-2-methyl-
There total 3 articles about Benzenecarboximidoyl chloride, N-hydroxy-2-methyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 50 percent / hydroxylamine hydrochloride, 50percent NaOH / ethanol; H2O / 1 h / 25 - 30 °C
2: N-chlorosuccinimide, HCl gas / dimethylformamide
With
hydrogenchloride; sodium hydroxide; N-chloro-succinimide; hydroxylamine hydrochloride;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo01307a039
- Guidance literature:
-
Multi-step reaction with 3 steps
1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride; potassium carbonate / dichloromethane / 18 h / 20 °C / Inert atmosphere
3: N-chloro-succinimide / dichloromethane; N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere
With
N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; hydroxylamine hydrochloride; potassium carbonate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0039-1690102