Oxiranecarboxylic acid, 3,3-diphenyl-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Oxiranecarboxylic acid, 3,3-diphenyl-, 1,1-dimethylethyl ester
• CAS No.: 75591-39-8
• Molecular Formula: C19H20O3
• Molecular Weight: 296.366
• Mol file: 75591-39-8.mol

Synonyms:

Chemical Property of Oxiranecarboxylic acid, 3,3-diphenyl-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Oxiranecarboxylic acid, 3,3-diphenyl-, 1,1-dimethylethyl ester

There total 1 articles about Oxiranecarboxylic acid, 3,3-diphenyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.6%

benzophenone (119-61-9) + tert-Butyl chloroacetate (107-59-5) → tert-butyl 3,3-diphenyl-oxirane-2-carboxylate (75591-39-8)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide;

Reference yield:

tert-butyl 3,3-diphenyl-oxirane-2-carboxylate (75591-39-8) → sodium 2,3-epoxy-3,3-diphenylpropionate (54934-19-9)

Guidance literature:

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; at 10 - 15 ℃;

DOI:10.1016/S0040-4039(03)00234-X

upstream raw materials:

benzophenone

tert-Butyl chloroacetate

Downstream raw materials:

sodium 2,3-epoxy-3,3-diphenylpropionate

Refernces

• 1、 Bansal, R. K.,Sethi, K.,Bachelor, F. W.. "Mass Spectrometric Studies of t-Butyl β-Phenylglycidates". . p. 515 - 517. Retrieved 2007/10/02.