N-[4-(2-chloroacetyl)phenyl]methanesulfonamide

Base Information Edit

Chemical Name:N-[4-(2-chloroacetyl)phenyl]methanesulfonamide
CAS No.:64488-52-4
Molecular Formula:C9H10 Cl N O3 S
Molecular Weight:247.702
Hs Code.:2935009090
European Community (EC) Number:613-606-0
DSSTox Substance ID:DTXSID0070102
Nikkaji Number:J453.269D
Wikidata:Q72516893
Mol file:64488-52-4.mol

Synonyms:64488-52-4;N-[4-(2-chloroacetyl)phenyl]methanesulfonamide;N-(4-(2-Chloroacetyl)phenyl)methanesulfonamide;Methanesulfonamide, N-[4-(chloroacetyl)phenyl]-;N-(p-Chloroacetylphenyl)methanesulfonamide;EC 613-606-0;Methanesulfonamide, N-(4-(chloroacetyl)phenyl)-;Methanesulfonamide, N-(4-(2-chloroacetyl)phenyl)-;N-[4-(2-chloro-1-oxoethyl)phenyl]methanesulfonamide;SCHEMBL3875386;DTXSID0070102;MFCD00144999;AKOS001094625;4'-(Mesylamino)-alpha-chloroacetophenone;AM804190;AS-54986;CS-0224276;FT-0640955;N-[4-(chloroacetyl)phenyl]methanesulfonamide;EN300-11859;4-(2-CHLOROACETYL)-METHANESULFONANILIDE;4-(2-CHLOROACETYL)-METHYLSULPHONANILIDE;W11787;A834773;AI-942/25034667;SR-01000062994;N-[4-(2-chloranylethanoyl)phenyl]methanesulfonamide;SR-01000062994-1;N-[4-(2- chloro-1-oxoethyl)phenyl]methanesulfonamide;Z57984666

Suppliers and Price of N-[4-(2-chloroacetyl)phenyl]methanesulfonamide

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
1g
$ 200.00

Matrix Scientific
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
500mg
$ 237.00

Crysdot
N-(4-(2-Chloroacetyl)phenyl)methanesulfonamide 95+%
5g
$ 280.00

Crysdot
N-(4-(2-Chloroacetyl)phenyl)methanesulfonamide 95+%
10g
$ 480.00

Crysdot
N-(4-(2-Chloroacetyl)phenyl)methanesulfonamide 95+%
1g
$ 80.00

Biosynth Carbosynth
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
500 mg
$ 150.00

Biosynth Carbosynth
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
250 mg
$ 85.00

Biosynth Carbosynth
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
2 g
$ 434.00

Biosynth Carbosynth
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
5 g
$ 868.00

Biosynth Carbosynth
N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide
1 g
$ 255.00

Total 69 raw suppliers

Chemical Property of N-[4-(2-chloroacetyl)phenyl]methanesulfonamide Edit

Chemical Property:

Vapor Pressure:6.06E-07mmHg at 25°C
Melting Point:197.5-199.0 °C
Boiling Point:410.4 °C at 760 mmHg
PKA:6.94±0.10(Predicted)
Flash Point:202 °C
PSA：71.62000
Density:1.433 g/cm³
LogP:2.63340
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:247.0069920
Heavy Atom Count:15
Complexity:315

Purity/Quality:

99% ^*data from raw suppliers

N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)NC1=CC=C(C=C1)C(=O)CCl
Uses N-[4-(2-Chloroacetyl)phenyl]methanesulfonamide, is a building block used in the synthesis of various compounds.

Technology Process of N-[4-(2-chloroacetyl)phenyl]methanesulfonamide

There total 4 articles about N-[4-(2-chloroacetyl)phenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1197-22-4
N-phenylmethanesulfonamide

: 79-04-9
chloroacetyl chloride

: 64488-52-4
N-[4-(2-chloro-1-oxoethyl)phenyl]methanesulfonamide

Guidance literature:: With aluminium trichloride; In dichloromethane; at -10 - 20 ℃; for 7h;
DOI:10.1021/jm00387a020

Reference yield:

: 62-53-3
aniline

: 64488-52-4
N-[4-(2-chloro-1-oxoethyl)phenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / pyridine / CH₂Cl₂ / 12 h / 20 °C

2: 75 percent / AlCl₃ / CH₂Cl₂ / 6 h / 20 °C

With pyridine; aluminium trichloride; In dichloromethane;
DOI:10.1016/j.bmcl.2004.05.084