N-(4-DIETHYLAMINOPHENYL)FORMAMIDE 97

Base Information

• Chemical Name: N-(4-DIETHYLAMINOPHENYL)FORMAMIDE 97
• CAS No.: 5235-68-7
• Molecular Formula: C11H16 N2 O
• Molecular Weight: 192.261
• Hs Code.: 2924299090
• Mol file: 5235-68-7.mol

Synonyms:Formanilide,4'-(diethylamino)- (6CI,7CI,8CI); NSC 522034

Chemical Property of N-(4-DIETHYLAMINOPHENYL)FORMAMIDE 97

Chemical Property:

• Vapor Pressure: 1.35E-05mmHg at 25°C
• Melting Point: 59-63 °C(lit.)
• Boiling Point: 367.6°C at 760 mmHg
• Flash Point: 176.1°C
• PSA: 32.34000
• Density: 1.084g/cm³
• LogP: 2.81000

Purity/Quality:

99% ^*data from raw suppliers

N-(4-DIETHYLAMINOPHENYL)FORMAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36/37/38-42/43
• Safety Statements: 26-36/37-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of N-(4-DIETHYLAMINOPHENYL)FORMAMIDE 97

There total 1 articles about N-(4-DIETHYLAMINOPHENYL)FORMAMIDE 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-diethylaniline (93-05-0) + formic acid ethyl ester (109-94-4) → N-(4-(diethylamino)phenyl)formamide (5235-68-7)

Guidance literature:

Heating;

Reference yield: 90.0%

N-(4-(diethylamino)phenyl)formamide (5235-68-7) → p-(diethylamino)phenyl isocyanide (42549-09-7)

Guidance literature:

With diisopropylamine; trichlorophosphate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.03.122

Reference yield: 64.0%

4-fluoro-1-iodobenzene (352-34-1) + N-(4-(diethylamino)phenyl)formamide (5235-68-7) → N-(4-(diethylamino)phenyl)-N-(4-fluorophenyl)formamide (1444155-36-5)

Guidance literature:

With copper(l) iodide; cesium fluoride; N,N`-dimethylethylenediamine; In tetrahydrofuran; Inert atmosphere; Reflux; Darkness;

DOI:10.1021/ja402566w

upstream raw materials:

N,N-diethylaniline

formic acid ethyl ester

Downstream raw materials:

p-(diethylamino)phenyl isocyanide

N-(4-(diethylamino)phenyl)-N-formyl-2-(thiophen-2-yl)acetamide

N-(4-(diethylamino)phenyl)-N-formyl-2-(naphthalen-1-yl)acetamide

N-(4-(diethylamino)phenyl)-N-(4-fluorophenyl)formamide