LABOTEST-BB LT00007814

Base Information

• Chemical Name: LABOTEST-BB LT00007814
• CAS No.: 79296-92-7
• Molecular Formula: C24H21NP.Cl
• Molecular Weight: 389.864
• Hs Code.: 2933399090
• Mol file: 79296-92-7.mol

Synonyms:pyridin-3-ylmethyltriphenylphosphonium chloride;triphenyl-(pyridin-3-yl-methyl)-phosphonium chloride;Phosphonium,triphenyl(3-pyridinylmethyl)-,chloride;triphenyl(3-pyridylmethyl)phosphine,chloride;(3-pyridyl)methyltriphenylphosphonium chloride;

Chemical Property of LABOTEST-BB LT00007814

Chemical Property:

• PSA: 26.48000
• LogP: 1.57970

Purity/Quality:

97% ^*data from raw suppliers

(3-PYRIDINYLMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of LABOTEST-BB LT00007814

There total 5 articles about LABOTEST-BB LT00007814 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-chloromethylpyridinium chloride (6959-48-4) + triphenylphosphine (603-35-0) → Triphenyl-3-pyridylmethylphosphonium chloride hydrochlorides (79296-92-7)

Guidance literature:

In N,N-dimethyl-formamide; at 140 ℃; for 20h;

DOI:10.1016/S0040-4039(01)90414-9

Reference yield: 68.0%

nicotinyl chloride (3099-31-8) + triphenylphosphine (603-35-0) → triphenyl-(pyridin-3-yl-methyl)-phosphonium chloride (79296-92-7)

Guidance literature:

In acetonitrile; for 30h; Heating;

Reference yield: 48.0%

triphenylphosphine (603-35-0) → triphenyl-(pyridin-3-yl-methyl)-phosphonium chloride (79296-92-7)

Guidance literature:

3-chloromethylpyridinium chloride; With potassium carbonate; In water;

triphenylphosphine; In xylene; at 133 - 134 ℃;

upstream raw materials:

nicotinyl chloride

triphenylphosphine

3-chloromethylpyridinium chloride

Downstream raw materials:

3-[2-(4-chloro-3-nitrophenyl)vinyl]pyridine

3-[2-(4-methylphenyl)ethenyl]pyridine

methyl 8-(p-chlorophenylsulfonamido)-4-[3-(pyridin-3-yl)-2-propenyl]-octanoate

2-Hydroxy-5-(2-pyridin-3-yl-ethyl)-benzaldehyde

Refernces

• 1、 -. "INDENE DERIVATIVES AS PHARMACEUTICAL AGENTS". Page 132. . Retrieved 2008/06/13.
• 2、 Doria,Passarotti,Sala,Magrini,Sberze,Tibolla,Ceserani,Castello. "Synthesis and antiulcer activity of (E)-5-[2-(3-pyridyl)ethenyl]-1H,7H-pyrazolo [1,5-a]pyrimidine-7-ones.". . p. 417 - 429. Retrieved 2007/10/02.