N'-Butyl-N,N-diethyl-1-phenylboranediamine

Base Information

• Chemical Name: N'-Butyl-N,N-diethyl-1-phenylboranediamine
• CAS No.: 79867-03-1
• Molecular Formula: C₁₄H₂₅BN₂
• Molecular Weight: 232.177
• DSSTox Substance ID: DTXSID90508343
• Wikidata: Q82365178
• Mol file: 79867-03-1.mol

Synonyms:79867-03-1;N'-Butyl-N,N-diethyl-1-phenylboranediamine;DTXSID90508343

Chemical Property of N'-Butyl-N,N-diethyl-1-phenylboranediamine

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 8
• Exact Mass: 232.2110790
• Heavy Atom Count: 17
• Complexity: 177

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: B(C1=CC=CC=C1)(NCCCC)N(CC)CC

Technology Process of N'-Butyl-N,N-diethyl-1-phenylboranediamine

There total 1 articles about N'-Butyl-N,N-diethyl-1-phenylboranediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

phenyl(chloro)(Et2)aminoborane (33441-65-5) + N-butylamine (109-73-9,85404-21-3) → n-butylamino(diethylamino)phenylborane (79867-03-1)

Guidance literature:

With triethylamine; In benzene; byproducts: NEt4Cl; B-compd. dissolved in benzene, cooled in ice bath, n-butylamine dissolved in benzene added dropwise with stirring, mixt. allowed to attain roomtemp., triethylamine added to resulted complex, mixt. refluxed for 3 h; NEt4Cl filtered, solvent removed from the filtrate, residue vac. distd.; elem. anal.;

DOI:10.1016/S0022-328X(00)93444-2

upstream raw materials:

phenyl(chloro)(Et₂)aminoborane

N-butylamine

Refernces