Technology Process of Phosphoric acid, mono(2-bromoethyl)
mono[3-(octadecyloxy)-2-(phenylmethoxy)propyl] ester, (R)-
There total 8 articles about Phosphoric acid, mono(2-bromoethyl)
mono[3-(octadecyloxy)-2-(phenylmethoxy)propyl] ester, (R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium chloride; triethylamine;
Yield given. Multistep reaction;
1.) CHCl3, room temp., 6h; 40 deg C, 12 h; 2.) 1 h;
DOI:10.1248/cpb.33.572
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / KH (22percent) / benzene / 2 h / Heating
2: 95 percent / HCl (2N) / tetrahydrofuran / 3 h / Ambient temperature
3: 1.) Pb(OAc)4; 2.) NaBH4 / 1.) benzene, 2 h, room temp.; 2.) methanol, THF, room temp.
4: 1.) NEt3; 2.) KCl (0.1N) / 1.) CHCl3, room temp., 6h; 40 deg C, 12 h; 2.) 1 h
With
lead(IV) acetate; hydrogenchloride; sodium tetrahydroborate; potassium chloride; potassium hydride; triethylamine;
In
tetrahydrofuran; benzene;
DOI:10.1248/cpb.33.572
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / p-toluenesulfonic acid monohydrate / 1 h / Heating
2: 94 percent / KH (22percent) / benzene / 2 h / Heating
3: 95 percent / HCl (2N) / tetrahydrofuran / 3 h / Ambient temperature
4: 1.) Pb(OAc)4; 2.) NaBH4 / 1.) benzene, 2 h, room temp.; 2.) methanol, THF, room temp.
5: 1.) NEt3; 2.) KCl (0.1N) / 1.) CHCl3, room temp., 6h; 40 deg C, 12 h; 2.) 1 h
With
lead(IV) acetate; hydrogenchloride; sodium tetrahydroborate; potassium chloride; potassium hydride; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; benzene;
DOI:10.1248/cpb.33.572