Phosphorous acid, 2,2-dimethylpropyl diphenyl ester

Base Information

• Chemical Name: Phosphorous acid, 2,2-dimethylpropyl diphenyl ester
• CAS No.: 80705-49-3
• Molecular Formula: C17H21O3P
• Molecular Weight: 304.326
• Mol file: 80705-49-3.mol

Synonyms:

Chemical Property of Phosphorous acid, 2,2-dimethylpropyl diphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphorous acid, 2,2-dimethylpropyl diphenyl ester

There total 5 articles about Phosphorous acid, 2,2-dimethylpropyl diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2,2-dimethyl-propanol-1 (75-84-3) + Diphenyl phosphorochloridite (5382-00-3) → neopentyl diphenyl phosphite (80705-49-3)

Guidance literature:

With pyridine; In Petroleum ether; for 312h; Ambient temperature;

DOI:10.1039/P29830001363

Reference yield:

dineopentyl phenyl phosphite (80733-03-5) → triphenyl phosphite (101-02-0) + diphenyl methylphosphonate (7526-26-3) + Methyl-phosphonic acid 2,2-dimethyl-propyl ester phenyl ester (88065-74-1) + neopentyl diphenyl phosphite (80705-49-3)

Guidance literature:

With methyl iodide; In neat (no solvent); at 33 ℃; for 1080h; Title compound not separated from byproducts;

DOI:10.1039/P29830001363

Reference yield:

dineopentyl phenyl phosphite (80733-03-5) + methyl iodide (74-88-4) → triphenyl phosphite (101-02-0) + diphenyl methylphosphonate (7526-26-3) + Methyl-phosphonic acid 2,2-dimethyl-propyl ester phenyl ester (88065-74-1) + neopentyl diphenyl phosphite (80705-49-3)

Guidance literature:

In neat (no solvent); at 33 ℃; for 1080h; Title compound not separated from byproducts;

DOI:10.1039/P29830001363

upstream raw materials:

2,2-dimethyl-propanol-1

Diphenyl phosphorochloridite

dineopentyl phenyl phosphite

methyl iodide

Downstream raw materials:

dineopentyl methylphosphonate

Methyl-phosphonic acid 2,2-dimethyl-propyl ester phenyl ester

dineopentyl phenyl phosphite

neopentyl phosphorodichloridite

Refernces