N,N',N''-tribenzylphosphorothioic triamide

Base Information

• Chemical Name: N,N',N''-tribenzylphosphorothioic triamide
• CAS No.: 53820-05-6
• Molecular Formula: C21H24N3PS
• Molecular Weight: 381.481
• NSC Number: 203102
• DSSTox Substance ID: DTXSID30308329
• Wikidata: Q82056144
• Mol file: 53820-05-6.mol

Synonyms:53820-05-6;N,N',N''-tribenzylphosphorothioic triamide;NSC203102;DTXSID30308329;NSC-203102

Chemical Property of N,N',N''-tribenzylphosphorothioic triamide

Chemical Property:

• Boiling Point: 542.4°Cat760mmHg
• Flash Point: 281.8°C
• Density: 1.197g/cm³
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 381.14285595
• Heavy Atom Count: 26
• Complexity: 365

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CNP(=S)(NCC2=CC=CC=C2)NCC3=CC=CC=C3

Technology Process of N,N',N''-tribenzylphosphorothioic triamide

There total 8 articles about N,N',N''-tribenzylphosphorothioic triamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-diphenyl-diamidodithiophosphoric acid (70578-12-0) + benzylamine (100-46-9) → N,N',N''-tribenzyl-thiophosphamide (53820-05-6) + aniline (62-53-3)

Guidance literature:

at 150 ℃;

DOI:10.1021/ja01187a022

Reference yield:

benzylamine (100-46-9) → N,N',N''-tribenzyl-thiophosphamide (53820-05-6)

Guidance literature:

With phosphorous (V) sulfide; at 180 ℃;

DOI:10.1021/ja01182a092

Reference yield:

tetraphosphorus decasulfide (15857-57-5) + benzylamine (100-46-9) → N,N',N''-tribenzyl-thiophosphamide (53820-05-6)

Guidance literature:

In not given; react. at elevated temp.;;

DOI:10.1021/ja01122a073

upstream raw materials:

N,N',N''-tripropyl-thiophosphamide

benzylamine

N,N',N''-trisphenylthiophosphoramide

2,4-dianilino-1,3-diphenyl-cyclodiphosphazane-2,4-disulfide

Refernces