1-Decanesulfonyl chloride

Base Information

• Chemical Name: 1-Decanesulfonyl chloride
• CAS No.: 61652-81-1
• Molecular Formula: C10H21ClO2S
• Molecular Weight: 240.795
• Hs Code.: 2904909090
• European Community (EC) Number: 634-717-0
• DSSTox Substance ID: DTXSID3069483
• Nikkaji Number: J429.430K
• Wikidata: Q81996382
• Mol file: 61652-81-1.mol

Synonyms:1-Decanesulfonyl chloride;61652-81-1;decane-1-sulfonyl chloride;1-Decanesulfonylchloride;decanesulfonylchloride;decanesulfonyl chloride;(Decylsulfonyl) chloride;1-Decanesulphonylchloride;C10H21ClO2S;SCHEMBL741780;DTXSID3069483;C10-H21-Cl-O2-S;MFCD00051746;1-Decanesulfonyl chloride, AldrichCPR;AKOS009158940;AS-58610;CS-0297535;FT-0607688;FT-0607689;EN300-680994

Chemical Property of 1-Decanesulfonyl chloride

Chemical Property:

• Vapor Pressure: 0.00109mmHg at 25°C
• Melting Point: 34oC
• Boiling Point: 310.5°Cat760mmHg
• Flash Point: 141.6°C
• PSA: 42.52000
• Density: 1.065g/cm³
• LogP: 4.77650
• Sensitive.: Moisture Sensitive
• Water Solubility.: It reacts with water.
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 9
• Exact Mass: 240.0950788
• Heavy Atom Count: 14
• Complexity: 207

Purity/Quality:

99% ^*data from raw suppliers

1-DECANESULPHONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 1771852
• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCS(=O)(=O)Cl
• Uses: 1-Decanesulfonyl chloride is used as pharmaceutical intermediate.

Technology Process of 1-Decanesulfonyl chloride

There total 4 articles about 1-Decanesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

didecyl disulfide (10496-18-1) → 1-decanesulfonyl chloride (61652-81-1)

Guidance literature:

With N-chloro-succinimide; In water; acetonitrile; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2014.02.013

Reference yield:

1-bromo dodecane (112-29-8) → 1-decanesulfonyl chloride (61652-81-1)

Guidance literature:

With water; sodium sulfite; at 200 ℃; Behandeln des Reaktionsprodukts mit Phosphor(V)-chlorid;

Reference yield:

1-thiocyanatodecane (5349-20-2) → 1-decanesulfonyl chloride (61652-81-1)

Guidance literature:

1-thiocyanatodecane; With water; acetic acid; at 50 ℃; for 0.5h;

With sulfuryl dichloride; at 50 ℃; for 0.5h;

DOI:10.1002/hc.20559

upstream raw materials:

1-bromo dodecane

1-thiocyanatodecane

didecyl disulfide

Downstream raw materials:

decane-1-sulfonanilide

perfluorodecane sulfonylfluoride

(4-Decansulfonamidobenzoyl)hydrazin

N'-(decylsulfonyloxy)-4-nitrobenzimidamide

Refernces

• 1、 Benfodda, Zohra,Guillen, Franck,Arnion, Helene,Dahmani, Abdelkader,Blancou, Hubert. "A new synthesis of alkane and polyfluoroalkanesulfonyl chlorides". experimental part. p. 355 - 361. Retrieved 2010/07/16.
• 2、 -. "N-sulfonyl-N-dihalophenylimidazolidinediones". . . Retrieved 2008/06/13.