Technology Process of Benzoic acid, 4,4'-dithiobis[2-chloro-, diethyl ester
There total 5 articles about Benzoic acid, 4,4'-dithiobis[2-chloro-, diethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 98 percent / H2 / Pd/C / ethyl acetate / 20 °C / 760 Torr
2.1: aq. HCl / 70 °C
2.2: NaNO2 / 0.33 h / 0 °C
2.3: 80 °C
3.1: aq. KOH / ethanol / 8 h / 80 °C
3.2: HCl / ethanol / 0 °C / pH 5
4.1: 1.34 g / aq. H2O2 / ethanol / 24 h / 20 °C
5.1: NaHCO3 / N,N-dimethyl-acetamide / 120 h / 20 °C
With
hydrogenchloride; potassium hydroxide; hydrogen; dihydrogen peroxide; sodium hydrogencarbonate;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl acetamide; ethyl acetate;
DOI:10.1021/jm040144e
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
N,N-dimethyl acetamide;
at 20 ℃;
for 120h;
DOI:10.1021/jm040144e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aq. HCl / 70 °C
1.2: NaNO2 / 0.33 h / 0 °C
1.3: 80 °C
2.1: aq. KOH / ethanol / 8 h / 80 °C
2.2: HCl / ethanol / 0 °C / pH 5
3.1: 1.34 g / aq. H2O2 / ethanol / 24 h / 20 °C
4.1: NaHCO3 / N,N-dimethyl-acetamide / 120 h / 20 °C
With
hydrogenchloride; potassium hydroxide; dihydrogen peroxide; sodium hydrogencarbonate;
In
ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jm040144e