Technology Process of 1-Butyl-3-(4-formylphenyl)sulfonylurea
There total 6 articles about 1-Butyl-3-(4-formylphenyl)sulfonylurea which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
1.) 0 deg C, 5 h; 2.) rt., overnight;
DOI:10.1248/cpb.31.2518
- Guidance literature:
-
With
SoLo-D241G unspecific peroxygenase; dihydrogen peroxide; ascorbic acid;
In
aq. phosphate buffer; acetonitrile;
at 30 ℃;
for 1h;
pH=7;
Reagent/catalyst;
Catalytic behavior;
Enzymatic reaction;
DOI:10.1016/j.tet.2019.02.013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 64 percent / potassium carbonate / tetrahydrofuran / Heating
2: 80 percent / lithium aluminium hydride / tetrahydrofuran / 1.) -78 deg C, 6 h; 2.) 0 deg C, overnight
3: 75 percent / pyridinium chlorochromate / CH2Cl2 / 1.) 0 deg C, 5 h; 2.) rt., overnight
With
lithium aluminium tetrahydride; potassium carbonate; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.31.2518
