4-(benzylsulfanyl)benzoic acid

Base Information Edit

Chemical Name:4-(benzylsulfanyl)benzoic acid
CAS No.:22855-95-4
Molecular Formula:C14H12 O2 S
Molecular Weight:244.314
Hs Code.:
Mol file:22855-95-4.mol

Synonyms:Benzoicacid, p-(benzylthio)- (8CI); 4-(Benzylthio)benzoic acid; NSC 212201;p-(Benzylthio)benzoic acid

Suppliers and Price of 4-(benzylsulfanyl)benzoic acid

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 4-(benzylsulfanyl)benzoic acid Edit

Chemical Property:

Vapor Pressure:6.28E-08mmHg at 25°C
Boiling Point:423.5°Cat760mmHg
Flash Point:209.9°C
Density:1.27g/cm³

Purity/Quality:: 99%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(benzylsulfanyl)benzoic acid

There total 10 articles about 4-(benzylsulfanyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 586-76-5
4-Bromobenzoic acid

: 100-39-0
benzyl bromide

: 22855-95-4
4-benzylsulfanylbenzoic acid

Guidance literature:: 4-Bromobenzoic acid; With tert.-butyl lithium; isopropylmagnesium chloride; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h;

benzyl bromide; With sulfur; at -78 - 20 ℃;
DOI:10.1016/j.tetlet.2006.07.056

Reference yield: 88.0%

: 1074-36-8
4-mercaptobenzoic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 22855-95-4
4-benzylsulfanylbenzoic acid

Guidance literature:: With water; palladium diacetate; sodium 3-(diphenylphosphanyl)benzenesulfonate; at 120 ℃; for 24h; chemoselective reaction;
DOI:10.1039/c2ob25091h

Reference yield: 80.0%

: 100-44-7
benzyl chloride

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 22855-95-4
4-benzylsulfanylbenzoic acid

Guidance literature:: benzyl chloride; With [2,2]bipyridinyl; copper(ll) sulfate pentahydrate; sodium thiosulfate pentahydrate; In methanol; water; at 80 ℃; for 2h; Schlenk technique;

4-amino-benzoic acid; With tert.-butylnitrite; In methanol; water; at 0 - 80 ℃; for 4.66667h; Schlenk technique;
DOI:10.1021/ol5009747