Propanoic acid, 2,2-dimethyl-, 4-formyl-1,2-phenylene ester

Base Information Edit

Chemical Name:Propanoic acid, 2,2-dimethyl-, 4-formyl-1,2-phenylene ester
CAS No.:84260-69-5
Molecular Formula:C17H22O5
Molecular Weight:306.359
Hs Code.:
Mol file:84260-69-5.mol

Synonyms:

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Chemical Property of Propanoic acid, 2,2-dimethyl-, 4-formyl-1,2-phenylene ester Edit

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MSDS Files:: SDS file from LookChem

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Technology Process of Propanoic acid, 2,2-dimethyl-, 4-formyl-1,2-phenylene ester

There total 1 articles about Propanoic acid, 2,2-dimethyl-, 4-formyl-1,2-phenylene ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3282-30-2
pivaloyl chloride

: 139-85-5
3,4-dihydroxybenzaldehyde

: 84260-69-5
4-formyl-1,2-phenylene bis(2,2-dimethylpropanoate)

Guidance literature:: With triethylamine; In tetrahydrofuran; at 25 ℃; for 3h;
DOI:10.1002/hlca.19910740216

Reference yield: 97.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1072879-54-9
3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine

: 84260-69-5
4-formyl-1,2-phenylene bis(2,2-dimethylpropanoate)

: 4-((2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-(ethoxycarbonyl)aziridin-2-yl)-1,2-phenylene bis(2,2-dimethylpropanoate)

Guidance literature:: 3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine; With triphenylborane; (R)-2,2’-diphenyl-(4-biphenanthrol); In toluene; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

diazoacetic acid ethyl ester; 4-formyl-1,2-phenylene bis(2,2-dimethylpropanoate); In toluene; at 20 ℃; for 20h; Inert atmosphere; Schlenk technique; Molecular sieve;
DOI:10.1021/jo501694h