Technology Process of Bis(4-methoxyphenyl)diazomethane
There total 6 articles about Bis(4-methoxyphenyl)diazomethane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
dichloromethane;
at 20 ℃;
for 4.5h;
DOI:10.1021/jm0204800
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 83 percent / hydrazine hydrate / ethanol / 48 h / Heating
2: 100 percent / MnO2 / CH2Cl2 / 4.5 h / 20 °C
With
manganese(IV) oxide; hydrazine hydrate;
In
ethanol; dichloromethane;
DOI:10.1021/jm0204800
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NH2NH2*H2O / 24 h / Heating
2: HgO, Na2SO4, ethanolic KOH / tetrahydrofuran / 0.75 h / Ambient temperature
With
potassium hydroxide; hydrazine hydrate; sodium sulfate; mercury(II) oxide;
In
tetrahydrofuran;
DOI:10.1021/jo00068a039
