Succinic acid hydrogen 1-[1-(1-adamantyl)propyl] ester

Base Information

• Chemical Name: Succinic acid hydrogen 1-[1-(1-adamantyl)propyl] ester
• CAS No.: 15037-74-8
• Molecular Formula: C17H26O4
• Molecular Weight: 294.3859
• Mol file: 15037-74-8.mol

Synonyms:Succinic acid mono-(1-adamantan-1-yl-propyl) ester;1-[1-(3-Carboxy-propionyloxy)-propyl]-adamantan;

Chemical Property of Succinic acid hydrogen 1-[1-(1-adamantyl)propyl] ester

Chemical Property:

• Vapor Pressure: 1.49E-08mmHg at 25°C
• Boiling Point: 428.8°Cat760mmHg
• Flash Point: 151.6°C
• PSA: 63.60000
• Density: 1.175g/cm³
• LogP: 3.38940

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Succinic acid hydrogen 1-[1-(1-adamantyl)propyl] ester

There total 3 articles about Succinic acid hydrogen 1-[1-(1-adamantyl)propyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(adamantan-1-yl)propan-1-one (1660-05-5) → 1-<1-(3-Carboxy-propionyloxy)-propyl>-adamantan (15037-74-8)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: Py / 6 h / Heating

With pyridine; lithium aluminium tetrahydride; In diethyl ether;

Reference yield:

1-Adamantanecarbonyl chloride (2094-72-6) → 1-<1-(3-Carboxy-propionyloxy)-propyl>-adamantan (15037-74-8)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) Mg, CdCl₂, benzene, (ii) /BRN= 389960/

2: LiAlH₄ / diethyl ether

3: Py / 6 h / Heating

With pyridine; lithium aluminium tetrahydride; In diethyl ether;

Reference yield:

succinic acid anhydride (108-30-5) + α-ethyl-1-adamantanemethanol (18341-84-9) → 1-<1-(3-Carboxy-propionyloxy)-propyl>-adamantan (15037-74-8)

Guidance literature:

With pyridine; for 6h; Heating;

upstream raw materials:

succinic acid anhydride

α-ethyl-1-adamantanemethanol

1-(adamantan-1-yl)propan-1-one

1-Adamantanecarbonyl chloride