N,N-dimethyl-4-(2-phenylhydrazinyl)aniline

Base Information

• Chemical Name: N,N-dimethyl-4-(2-phenylhydrazinyl)aniline
• CAS No.: 63042-07-9
• Molecular Formula: C14H17N3
• Molecular Weight: 227.309
• Mol file: 63042-07-9.mol

Synonyms:

Chemical Property of N,N-dimethyl-4-(2-phenylhydrazinyl)aniline

Chemical Property:

• Vapor Pressure: 0.00104mmHg at 25°C
• Boiling Point: 301.7°Cat760mmHg
• Flash Point: 135.1°C
• Density: 1.17g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-dimethyl-4-(2-phenylhydrazinyl)aniline

There total 2 articles about N,N-dimethyl-4-(2-phenylhydrazinyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl yellow (60-11-7) → N,N-dimethyl-4-(N'-phenyl-hydrazino)-aniline (63042-07-9)

Guidance literature:

With Clostridium perfringens azoreductase; for 4h; stereospecific reaction; Darkness; Enzymatic reaction;

DOI:10.1016/j.bmcl.2012.10.014

Reference yield:

methyl yellow (60-11-7) → N,N-dimethyl-4-(N'-phenyl-hydrazino)-aniline (63042-07-9)

Guidance literature:

With ethanol; 2,2'-bis(trifluoromethyl)benzophenone; Quantum yield; Irradiation; var. sensitizers: benzophenone, 3,3'- and 4,4'-bis(trifluoromethyl)benzo;

DOI:10.1246/cl.1984.881

Reference yield: 90.0%

N,N-dimethyl-4-(N'-phenyl-hydrazino)-aniline (63042-07-9) → methyl yellow (60-11-7)

Guidance literature:

With trichloroisocyanuric acid; In tetrahydrofuran; at 20 ℃; for 0.216667h; Green chemistry;

DOI:10.1055/s-0039-1690052

upstream raw materials:

methyl yellow

methyl yellow

Downstream raw materials:

4-amino-N,N-dimethylaniline

aniline

methyl yellow

Refernces

• 1、 Ke, Xuebin,Sarina, Sarina,Zhao, Jian,Zhang, Xingguang,Chang, Jin,Zhu, Huaiyong. "Tuning the reduction power of supported gold nanoparticle photocatalysts for selective reductions by manipulating the wavelength of visible light irradiation". supporting information; experimental part. p. 3509 - 3511. Retrieved 2012/06/18.
• 2、 O'Dea, John J.,Osteryoung, Janet G.. "Square Wave Voltammetry for Two-Step Surface Reductions". . p. 650 - 658. Retrieved 2007/10/03.