N-ISOPROPYLHYDROXYLAMINE HYDROCHLORIDE

Base Information

• Chemical Name: N-ISOPROPYLHYDROXYLAMINE HYDROCHLORIDE
• CAS No.: 50632-53-6
• Molecular Formula: C3H10ClNO
• Molecular Weight: 111.572
• Hs Code.: 29280000
• Mol file: 50632-53-6.mol

Synonyms:Isopropylhydroxylaminehydrochloride;N-(2-Propyl)hydroxylamine hydrochloride;N-Hydroxy-2-propanaminehydrochloride;N-Isopropylhydroxylamine hydrochloride;

Chemical Property of N-ISOPROPYLHYDROXYLAMINE HYDROCHLORIDE

Chemical Property:

• Appearance/Colour: White to beige adhering crystalline powder
• Vapor Pressure: 16.5mmHg at 25°C
• Melting Point: 68-72 °C
• Boiling Point: 104.9 °C at 760 mmHg
• Flash Point: 44.5 °C
• PSA: 32.26000
• LogP: 1.56650
• Storage Temp.: −20°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-Isopropylhydroxylamine Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn,Xi
• Hazard Codes: Xn,Xi
• Statements: 22-36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-ISOPROPYLHYDROXYLAMINE HYDROCHLORIDE

There total 2 articles about N-ISOPROPYLHYDROXYLAMINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diisopropylamine (108-18-9) → N-isopropylhydroxylamine hydrochloride (50632-53-6)

Guidance literature:

diisopropylamine; With dihydrogen peroxide; In methanol; water; at 40 - 60 ℃; for 6.5h;

With hydrogenchloride; In methanol; water; at 50 ℃; for 5.5h; under 37.5038 - 112.511 Torr;

Reference yield:

2-nitropropane (79-46-9) → N-isopropylhydroxylamine hydrochloride (50632-53-6)

Guidance literature:

With ammonium chloride; zinc; In water; at 15 - 35 ℃;

DOI:10.1134/S003602361312005X

Reference yield: 100.0%

4-Trifluoromethylbenzaldehyde (455-19-6) + N-isopropylhydroxylamine hydrochloride (50632-53-6) → N-iso-propyl,α-(4-trifluoromethyl)phenyl nitrone (1353013-03-2)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 20 ℃; Inert atmosphere;

DOI:10.1039/c1ob06144e

upstream raw materials:

2-nitropropane

diisopropylamine

Downstream raw materials:

C₁₈H₂₁NO₃

2-Isopropyl-4-methyl-3,5-diphenylimino-1,2,4-oxadiazolidin

O-Benzoyl-N-isopropylhydroxylammoniumchlorid

C₃₉H₅₁N₇O₉

Refernces

• 1、 Beirakhov,Orlova,Il'In,Sakharov,Goeva,Churakov,Surazhskaya,Mikhailov. "Molybdenum(VI) complexes with N-substituted hydroxylamines". . p. 1446 - 1451. Retrieved 2014/01/23.