Benzoic acid, 2-hydroxy-, 1-methyl-3-hexynyl ester

Base Information

• Chemical Name: Benzoic acid, 2-hydroxy-, 1-methyl-3-hexynyl ester
• CAS No.: 873888-86-9
• Molecular Formula: C14H16O3
• Molecular Weight: 232.279
• Mol file: 873888-86-9.mol

Synonyms:

Chemical Property of Benzoic acid, 2-hydroxy-, 1-methyl-3-hexynyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-hydroxy-, 1-methyl-3-hexynyl ester

There total 1 articles about Benzoic acid, 2-hydroxy-, 1-methyl-3-hexynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(R,S)-4-Heptyn-2-ol (19781-81-8) + methyl salicylate (119-36-8,8024-54-2) → 4-heptyn-2-yl salicylate (873888-86-9)

Guidance literature:

titanium(IV)isopropoxide; In methanol; at 150 ℃; for 24h;

Reference yield: 88.0%

4-heptyn-2-yl salicylate (873888-86-9) → (Z)-4-hepten-2-yl salicylate (873888-84-7)

Guidance literature:

With hydrogen; Pd-BaSO₄; In ethanol; for 3h;

upstream raw materials:

(R,S)-4-Heptyn-2-ol

methyl salicylate

Downstream raw materials:

(Z)-4-hepten-2-yl salicylate

Refernces