Methyl tetrahydro-2,5-dimethoxyfuroate

Base Information

• Chemical Name: Methyl tetrahydro-2,5-dimethoxyfuroate
• CAS No.: 39658-49-6
• Molecular Formula: C8H14 O5
• Molecular Weight: 190.196
• European Community (EC) Number: 254-568-1
• DSSTox Substance ID: DTXSID60960272
• Nikkaji Number: J261.417K
• Mol file: 39658-49-6.mol

Synonyms:39658-49-6;METHYLTETRAHYDRO-2,5-DIMETHOXY-2-FURANCARBOXYLATE;methyl 2,5-dimethoxyoxolane-2-carboxylate;methyl 2,5-dimethoxytetrahydrofuran-2-carboxylate;Methyl tetrahydro-2,5-dimethoxyfuroate;EINECS 254-568-1;SCHEMBL2335332;DTXSID60960272;2-Furancarboxylic acid,tetrahydro-2,5-dimethoxy-, methyl ester;AKOS006272129;NS00057698;2-methoxycarbonyl-2,5-dimethoxytetrahydrofuran;EN300-7494370;methyl 2,5-dimethoxy-tetrahydrofuran-2-carboxylate;2,5-dimethoxy-tetrahydro-furan-2-carboxylic acid methyl ester

Chemical Property of Methyl tetrahydro-2,5-dimethoxyfuroate

Chemical Property:

• Vapor Pressure: 0.035mmHg at 25°C
• Boiling Point: 242.1°Cat760mmHg
• Flash Point: 99.8°C
• PSA: 53.99000
• Density: 1.14g/cm³
• LogP: 0.28500
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 4
• Exact Mass: 190.08412354
• Heavy Atom Count: 13
• Complexity: 193

Purity/Quality:

99% ^*data from raw suppliers

MethylTetrahydro-2,5-dimethoxy-2-furancarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1CCC(O1)(C(=O)OC)OC

Technology Process of Methyl tetrahydro-2,5-dimethoxyfuroate

There total 3 articles about Methyl tetrahydro-2,5-dimethoxyfuroate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-dimethoxy-2,5-dihydro-furan-2-carboxylic acid methyl ester (62435-72-7) → 2,5-dimethoxy-tetrahydro-furan-2-carboxylic acid methyl ester (39658-49-6)

Guidance literature:

With methanol; nickel; under 73550.8 Torr; Hydrogenation;

Reference yield:

2-furoic acid methyl ester (611-13-2) → 2,5-dimethoxy-tetrahydro-furan-2-carboxylic acid methyl ester (39658-49-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / Electrolysis

2: Raney nickel; methanol / 73550.8 Torr / Hydrogenation

With methanol; sulfuric acid; nickel;

Reference yield:

→ 2,5-dimethoxy-tetrahydro-furan-2-carboxylic acid methyl ester (39658-49-6)

Guidance literature:

aus Methyl-2,5-dihydro-2,5-dimethoxy-2-furoat, H2/Pd-C;

upstream raw materials:

2,5-dimethoxy-2,5-dihydro-furan-2-carboxylic acid methyl ester

2-furoic acid methyl ester

Downstream raw materials:

1-(2-chlorophenyl)-1H-pyrrole-2-carboxylic acid

Methyl 3,4,5-Tribromo-1-(2-p-tolylethyl)pyrrole-2-carboxylate

3,4,5-Tribromo-1-(2-p-tolyl-ethyl)-1H-pyrrole-2-carbonyl chloride

3,4,5-Tribromo-1-(2-p-tolyl-ethyl)-1H-pyrrole-2-carboxylic acid