1,10-Diacetoxydecane

Base Information

• Chemical Name: 1,10-Diacetoxydecane
• CAS No.: 26118-61-6
• Molecular Formula: C14H26 O4
• Molecular Weight: 258.358
• Hs Code.: 2915390090
• European Community (EC) Number: 247-471-0
• DSSTox Substance ID: DTXSID00885334
• Nikkaji Number: J25.607B
• Wikidata: Q82863953
• Mol file: 26118-61-6.mol

Synonyms:1,10-Diacetoxydecane;26118-61-6;1,10-Decanediol, diacetate;10-acetyloxydecyl acetate;Decamethylene diacetate;1,10-Decanediol, 1,10-diacetate;Decamethylene glycol diacetate;EINECS 247-471-0;AI3-06197;1,10-Decanediol Diacetate;Decane-1,10-diyl diacetate;SCHEMBL15299079;DTXSID00885334;10-(ACETYLOXY)DECYL ACETATE;MFCD03093628;AKOS025295014;AS-60570;CS-0450483;D2783;D90115

Chemical Property of 1,10-Diacetoxydecane

Chemical Property:

• Vapor Pressure: 0.00109mmHg at 25°C
• Melting Point: 26 °C
• Boiling Point: 300.9°Cat760mmHg
• Flash Point: 135°C
• PSA: 52.60000
• Density: 0.969g/cm³
• LogP: 3.23340
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 13
• Exact Mass: 258.18310931
• Heavy Atom Count: 18
• Complexity: 202

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,10-Diacetoxydecane >97.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCCCCCCCCCCOC(=O)C

Technology Process of 1,10-Diacetoxydecane

There total 21 articles about 1,10-Diacetoxydecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Isopropenyl acetate (108-22-5) + 1,10-Decanediol (112-47-0) → 1,10-decanediol diacetate (26118-61-6)

Guidance literature:

With iodine; at 85 - 90 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2006.05.122

Reference yield: 87.0%

1,10-Decanediol (112-47-0) + ethyl acetate (141-78-6) → 1,10-decanediol diacetate (26118-61-6)

Guidance literature:

With aluminum oxide; at 25 - 30 ℃; for 1h;

DOI:10.1055/s-1981-29594

Reference yield: 50.0%

1,2-di(tetrahydrofuran-2-yl)ethane (1793-98-2) + acetic acid (64-19-7,77671-22-8) → n-decyl acetate (112-17-4) + 1,10-decanediol diacetate (26118-61-6)

Guidance literature:

With palladium on activated charcoal; hydrogen; scandium tris(trifluoromethanesulfonate); at 185 ℃; for 1h; under 30003 Torr; Autoclave;

upstream raw materials:

1,10-Decanediol

acetyl chloride

mercury(II) diacetate

1,10-dibromodecane

Downstream raw materials:

1,10-decadiene

9-decen-1-yl acetate

Refernces

• 1、 Deng, Chen-Qiang,Jiang, Qin-Zhu,Deng, Jin,Fu, Yao. "Synthesis of 1,10-decanediol diacetate and 1-decanol acetate from furfural". . p. 2169 - 2176. Retrieved 2021/03/26.
• 2、 -. "Method for synthesizing 1,9-decadiene". Paragraph 0036-0038; 0068-0080. . Retrieved 2019/07/01.