Technology Process of 2-Azetidinone, 3-amino-1-(4-methoxyphenyl)-
There total 6 articles about 2-Azetidinone, 3-amino-1-(4-methoxyphenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
rhodium on alumina;
In
methanol;
under 4180 Torr;
Ambient temperature;
DOI:10.1021/ja00363a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) O3, 2.) Me2S / 1.) AcOEt, -78 deg C, 15 min, 2.) -78 deg C, 20 min
2: 61 percent / H2NOH*HCl, pyridine / methanol / 12 h / Ambient temperature
3: 75 percent / H2 / 5percent rhodium-alumina / methanol / 4180 Torr / Ambient temperature
With
pyridine; dimethylsulfide; hydroxylamine hydrochloride; hydrogen; ozone;
rhodium on alumina;
In
methanol;
DOI:10.1021/ja00363a023
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2.) KOH, n-Bu4NBr, H2O / 2.) C6H6, room temperature, 24 h
2: 99 percent / MCPBA / CH2Cl2 / 0.33 h / -78 °C
3: 78 percent / toluene / 20 h / Heating
4: 1.) O3, 2.) Me2S / 1.) AcOEt, -78 deg C, 15 min, 2.) -78 deg C, 20 min
5: 61 percent / H2NOH*HCl, pyridine / methanol / 12 h / Ambient temperature
6: 75 percent / H2 / 5percent rhodium-alumina / methanol / 4180 Torr / Ambient temperature
With
pyridine; potassium hydroxide; dimethylsulfide; hydroxylamine hydrochloride; tetrabutylammomium bromide; water; hydrogen; ozone; 3-chloro-benzenecarboperoxoic acid;
rhodium on alumina;
In
methanol; dichloromethane; toluene;
DOI:10.1021/ja00363a023