Technology Process of Benzamide, N,N-diethyl-2-methoxy-6-methyl-
There total 10 articles about Benzamide, N,N-diethyl-2-methoxy-6-methyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenylphosphine; lithium chloride;
bis-triphenylphosphine-palladium(II) chloride;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 8h;
DOI:10.1016/S0040-4039(00)73902-5
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine
2: 49 percent / LiCl, PPh3, PdCl2(PPh3)2 / dimethylformamide / 8 h / 120 °C
With
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride;
In
pyridine; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: K / tetrahydrofuran / 1.) room temperature, 12-18 h, 2.) -40 deg C, 2.5 h
2: 0.6 mol dm-3 HCl / methanol / 1 h / Ambient temperature
3: pyridine
4: 49 percent / LiCl, PPh3, PdCl2(PPh3)2 / dimethylformamide / 8 h / 120 °C
With
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium; triphenylphosphine; lithium chloride;
In
tetrahydrofuran; pyridine; methanol; N,N-dimethyl-formamide;