M-Iodobenzenesulphonyl chloride

Base Information

• Chemical Name: M-Iodobenzenesulphonyl chloride
• CAS No.: 50702-38-0
• Molecular Formula: C6H4 Cl I O2 S
• Molecular Weight: 302.52
• Hs Code.: 2904909090
• European Community (EC) Number: 818-955-4
• DSSTox Substance ID: DTXSID00198759
• Nikkaji Number: J1.619.653C
• Wikidata: Q72483375
• Mol file: 50702-38-0.mol

Synonyms:50702-38-0;3-iodobenzenesulfonyl chloride;M-IODOBENZENESULPHONYL CHLORIDE;3-iodobenzene-1-sulfonyl chloride;Benzenesulfonylchloride, 3-iodo-;Benzenesulfonyl chloride, 3-iodo-;m-Iodobenzenesulfonyl chloride;SCHEMBL486222;3-iodo-benzenesulfonyl chloride;(3-Iodophenyl)sulphonyl chloride;3-iodobenzene-1-sulfonylchloride;DTXSID00198759;PFIYKHNOMGYTGR-UHFFFAOYSA-N;MFCD06409087;AKOS009161326;BS-13459;CS-0245442;FT-0760545;EN300-30519

Chemical Property of M-Iodobenzenesulphonyl chloride

Chemical Property:

• Vapor Pressure: 0.000164mmHg at 25°C
• Boiling Point: 341℃
• Flash Point: 160℃
• PSA: 42.52000
• Density: 2.041
• LogP: 3.29950
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 301.86653
• Heavy Atom Count: 11
• Complexity: 221

Purity/Quality:

98%Min ^*data from raw suppliers

3-IODOBENZENE-1-SULFONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)I)S(=O)(=O)Cl

Technology Process of M-Iodobenzenesulphonyl chloride

There total 2 articles about M-Iodobenzenesulphonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-iodo-benzenesulfonic acid (50702-37-9) → 3-iodobenzenesulfonyl chloride (50702-38-0)

Guidance literature:

With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 45 ℃; for 2.5h;

Reference yield:

→ 3-iodobenzenesulfonyl chloride (50702-38-0)

Guidance literature:

With phosphorus pentachloride;

Reference yield: 100.0%

3-iodobenzenesulfonyl chloride (50702-38-0) + phenol (108-95-2,27073-41-2) → C12H9IO3S

Guidance literature:

phenol; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.166667h;

3-iodobenzenesulfonyl chloride; In dichloromethane; at 20 ℃;

upstream raw materials:

3-iodo-benzenesulfonic acid

Downstream raw materials:

3-Iodo-N-(3-methyl-2-pyridinyl)benzenesulfonamide

4-[(3-iodophenyl)sulfonyl]morpholine

3-iodo-N-methylbenzenesulfonamide

3-iod phenyl sulfonyl-Phe(3-CN)-OH

Refernces