Technology Process of N-Cyclohexyl-4-MethoxybenzaMide, 97%
There total 43 articles about N-Cyclohexyl-4-MethoxybenzaMide, 97% which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Bromotrichloromethane; 4-(diphenylphosphino)-benzyltrimethylammonium bromide; triethylamine;
In
tetrahydrofuran;
at 60 ℃;
for 6h;
Inert atmosphere;
DOI:10.1016/j.tet.2013.03.021
- Guidance literature:
-
4-methoxy-benzaldehyde;
With
sodium azide; trifluorormethanesulfonic acid; acetic acid;
at 40 ℃;
for 2h;
cyclohexanol;
With
trifluorormethanesulfonic acid;
at 90 ℃;
DOI:10.1016/j.tetlet.2016.08.069
- Guidance literature:
-
cyclohexylamine;
With
iodine; triphenylphosphine;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
terephthalic acid;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 0.25h;
Inert atmosphere;
DOI:10.1039/c5ra03184b
