2-O,3-O,4-O,5-O,6-O-Pentaacetyl-1-deoxo-D-galactose

Base Information

• Chemical Name: 2-O,3-O,4-O,5-O,6-O-Pentaacetyl-1-deoxo-D-galactose
• CAS No.: 7226-60-0
• Molecular Formula: C₁₆H₂₄O₁₀
• Molecular Weight: 376.361
• Mol file: 7226-60-0.mol

Synonyms:Penta-O-acetyl-1-desoxy-L-galactit;1-(pentane-1-sulfonyl)-pyrrolidine;Pentansulfonsaeure-pyrrolidid;penta-O-acetyl-1-deoxy-L-galactitol;1-Desoxy-D-galaktit-pentaacetat;

Chemical Property of 2-O,3-O,4-O,5-O,6-O-Pentaacetyl-1-deoxo-D-galactose

Chemical Property:

• Boiling Point: 333.4°Cat760mmHg
• Flash Point: 155.4°C
• PSA: 85.22000
• Density: g/cm³
• LogP: 2.46180

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-O,3-O,4-O,5-O,6-O-Pentaacetyl-1-deoxo-D-galactose

There total 7 articles about 2-O,3-O,4-O,5-O,6-O-Pentaacetyl-1-deoxo-D-galactose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetra-O-acetyl-D-xylose (3891-58-5,5139-19-5,30571-54-1,30571-57-4,64649-85-0,92218-64-9,92218-65-0,30571-56-3) → penta-O-acetyl-6-deoxy-L-glucitol (7208-41-5,7226-56-4,7226-57-5,7226-60-0,7226-63-3,7333-15-5,7333-28-0,7333-29-1,7333-30-4,51607-20-6,67335-79-9,67335-80-2,79466-33-4,82768-55-6,88853-38-7,94425-24-8,98975-53-2) + penta-O-acetyl-1-deoxy-D-iditol (7208-41-5,7226-56-4,7226-57-5,7226-60-0,7226-63-3,7333-15-5,7333-28-0,7333-29-1,7333-30-4,51607-20-6,67335-79-9,67335-80-2,79466-33-4,82768-55-6,88853-38-7,94425-24-8,98975-53-2)

Guidance literature:

With methyl magnesium iodide; diethyl ether; benzene; Behandeln des nach der Hydrolyse erhaltenen Reaktionsprodukts mit Acetanhydrid und Pyridin;

DOI:10.1021/ja01158a025

Reference yield:

tetra-O-acetyl-D-xylose (3891-58-5,5139-19-5,30571-54-1,30571-57-4,64649-85-0,92218-64-9,92218-65-0,30571-56-3) → penta-O-acetyl-6-deoxy-L-glucitol (7208-41-5,7226-56-4,7226-57-5,7226-60-0,7226-63-3,7333-15-5,7333-28-0,7333-29-1,7333-30-4,51607-20-6,67335-79-9,67335-80-2,79466-33-4,82768-55-6,88853-38-7,94425-24-8,98975-53-2) + penta-O-acetyl-1-deoxy-D-iditol (7208-41-5,7226-56-4,7226-57-5,7226-60-0,7226-63-3,7333-15-5,7333-28-0,7333-29-1,7333-30-4,51607-20-6,67335-79-9,67335-80-2,79466-33-4,82768-55-6,88853-38-7,94425-24-8,98975-53-2)

Guidance literature:

With methyl magnesium iodide; diethyl ether; benzene; Behandeln des nach der Hydrolyse erhaltenen Reaktionsprodukts mit Acetanhydrid und Pyridin;

DOI:10.1021/ja01158a025

Reference yield:

1-deoxy-D-iditol (123672-37-7) + acetic anhydride (108-24-7) → penta-O-acetyl-1-deoxy-D-iditol (7208-41-5,7226-56-4,7226-57-5,7226-60-0,7226-63-3,7333-15-5,7333-28-0,7333-29-1,7333-30-4,51607-20-6,67335-79-9,67335-80-2,79466-33-4,82768-55-6,88853-38-7,94425-24-8,98975-53-2)

Guidance literature:

With pyridine; at 100 ℃; for 0.25h;

DOI:10.1016/S0008-6215(00)90459-2

upstream raw materials:

L-fucitol

acetic anhydride

methyl iodide

tetra-O-acetyl-D-xylose

Downstream raw materials:

1-deoxy-D-gulitol

Refernces

• 1、 Voiland, Annie,Michel, Georges. "CHARACTERIZATION OF 6-DEOXY-D-ALTRITOL IN THE CELL-WALL POLYSACCHARIDE OF Nocardia asteroides R 399". . p. 283 - 288. Retrieved 2007/10/02.