Technology Process of 1,2-Bis[4-(benzyloxy)-3-methoxyphenyl]propane-1,3-diol
There total 11 articles about 1,2-Bis[4-(benzyloxy)-3-methoxyphenyl]propane-1,3-diol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
Ambient temperature;
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / potassium hydroxide / H2O; ethanol / 2 h
2: 79 percent / 35 percent hydrogen peroxide, 3 M sodium hydroxide, tetrabutylammonium hydrogen sulfate / CH2Cl2 / 1.) 0 deg C up to 16 deg C, 6 h
3: 1.) BF3*(C2H5)2O, 2.) sodium borohydride / 1.) ether, reflux, 30 min, 2.) tetrahydrofurane, 52 h
With
potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate;
In
ethanol; dichloromethane; water;