Octanoic acid, 2-pyridinyl ester

Base Information

• Chemical Name: Octanoic acid, 2-pyridinyl ester
• CAS No.: 89398-02-7
• Molecular Formula: C13H19NO2
• Molecular Weight: 221.299
• Mol file: 89398-02-7.mol

Synonyms:

Chemical Property of Octanoic acid, 2-pyridinyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Octanoic acid, 2-pyridinyl ester

There total 2 articles about Octanoic acid, 2-pyridinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,2'-dipyridyl carbonate (1659-31-0) + Octanoic acid (124-07-2) → 2-hydroxypyridin (142-08-5) + benzyl caprylate (10276-85-4) + 2-pyridyl caprylate (89398-02-7)

Guidance literature:

With benzyl alcohol; dmap; In dichloromethane; for 0.2h; Ambient temperature;

DOI:10.1016/S0040-4039(01)91265-1

Reference yield: 84.0%

2,2'-dipyridyl carbonate (1659-31-0) + Octanoic acid (124-07-2) + benzyl alcohol (100-51-6,185532-71-2) → 2-hydroxypyridin (142-08-5) + benzyl caprylate (10276-85-4) + 2-pyridyl caprylate (89398-02-7)

Guidance literature:

dmap; In dichloromethane; for 0.2h; Product distribution; Ambient temperature; investigation of reaction with various carboxylic acids and alcohols or thiols;

DOI:10.1016/S0040-4039(01)91265-1

Reference yield: 88.0%

2-pyridyl caprylate (89398-02-7) + tert-butyl alcohol (75-65-0) → tert-butyl octanoate (5457-66-9)

Guidance literature:

With copper(ll) bromide; In acetonitrile; at 80 ℃; for 0.5h;

DOI:10.1021/jo00184a009

upstream raw materials:

2,2'-dipyridyl carbonate

Octanoic acid

benzyl alcohol

Downstream raw materials:

tert-butyl octanoate

Refernces