2-IODOETHYL METHYL ETHER

Base Information

• Chemical Name: 2-IODOETHYL METHYL ETHER
• CAS No.: 4296-15-5
• Molecular Formula: C3H7IO
• Molecular Weight: 185.992
• Hs Code.: 2909199090
• Mol file: 4296-15-5.mol

Synonyms:Ether,2-iodoethyl methyl (6CI,7CI,8CI);1-Iodo-2-methoxyethane;2-Iodoethyl methylether;2-Methoxyethyl iodide;Methyl 2-iodoethyl ether;NSC 9228;

Chemical Property of 2-IODOETHYL METHYL ETHER

Chemical Property:

• Vapor Pressure: 10mmHg at 25°C
• Refractive Index: 1.505
• Boiling Point: 134.4 °C at 760 mmHg
• Flash Point: 35.1 °C
• PSA: 9.23000
• Density: 1.801 g/cm³
• LogP: 1.06780
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

99% ^*data from raw suppliers

1-Iodo-2-methoxy-ethane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-IODOETHYL METHYL ETHER

There total 12 articles about 2-IODOETHYL METHYL ETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-methoxy-ethyl p-toluenesulfonyloxy ester (17178-10-8,58320-73-3) → 2-iodo-1-methoxyethane (4296-15-5)

Guidance literature:

With sodium iodide; In acetone; at 20 ℃; for 24h; Inert atmosphere; Darkness;

DOI:10.1021/cm203790z

Reference yield: 66.0%

2-Bromoethyl methyl ether (6482-24-2) → 2-iodo-1-methoxyethane (4296-15-5)

Guidance literature:

With sodium iodide; In acetone; Reflux;

Reference yield:

2-chloroethyl methyl ether (627-42-9) → 2-iodo-1-methoxyethane (4296-15-5)

Guidance literature:

With acetone; sodium iodide;

upstream raw materials:

methanol

methyl hypoiodite

ethene

1,2-Diiodoethane

Downstream raw materials:

2'-O-(2-methoxyethyl)adenosine

1-[((2S,3S)-3-phenyloxiran-2-yl)methoxy]-2-methoxyethane

1-bromo-3-(2-methoxyethoxy)benzene

β-Cyanoethyl-2-methoxyethylphenylphosphine

Refernces

• 1、 Olah,G.A. et al.. "-". . p. 2587 - 2594. Retrieved 1968.
• 2、 -. "Substituted Oxopyridine Derivatives and Use Thereof in the Treatment of Cardiovascular Disorders". Paragraph 1196-1199. . Retrieved 2016/05/02.
• 3、 -. "SUBSTITUTED OXOPYRIDINE DERIVATIVES AND USE THEREOF IN THE TREATMENT OF CARDIOVASCULAR DISORDERS". Paragraph 1719-1722. . Retrieved 2016/10/07.