L-Proline, 1-L-leucyl-, phenylmethyl ester, monohydrochloride

Base Information Edit

Chemical Name:L-Proline, 1-L-leucyl-, phenylmethyl ester, monohydrochloride
CAS No.:89545-43-7
Molecular Formula:C18H26N2O3.ClH
Molecular Weight:354.877
Hs Code.:
Mol file:89545-43-7.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Proline, 1-L-leucyl-, phenylmethyl ester, monohydrochloride Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of L-Proline, 1-L-leucyl-, phenylmethyl ester, monohydrochloride

There total 7 articles about L-Proline, 1-L-leucyl-, phenylmethyl ester, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 83610-44-0
benzyl (2S)-1-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-4-methylpentanoyl]pyrrolidine-2-carboxylate

: 89545-43-7
H-Leu-Pro-OBzl hydrochloride

Guidance literature:: With hydrogenchloride; In neat (no solvent, solid phase); for 2h;
DOI:10.1039/c3gc40302e

Reference yield: 76.7%

: 132548-05-1
Nps-Leu-Pro-OBzl

: 89545-43-7
H-Leu-Pro-OBzl hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; ethyl acetate; at 20 ℃; for 0.166667h;

Reference yield:

: 16652-71-4
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride

: 89545-43-7
H-Leu-Pro-OBzl hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / Ambient temperature

2: 90 percent / HCl, formic acid / 0.5 h / Ambient temperature

With hydrogenchloride; formic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1246/bcsj.56.3329