Technology Process of 6-(5-{[5-cyano-1,4-dimethyl-2-(3-methylpiperidin-1-yl)-6-oxo-1,6-dihydropyridin-3-yl]methylidene}-4-oxo-2-thioxo-1,3-thiazolidin-3-yl)hexanoic acid
There total 11 articles about 6-(5-{[5-cyano-1,4-dimethyl-2-(3-methylpiperidin-1-yl)-6-oxo-1,6-dihydropyridin-3-yl]methylidene}-4-oxo-2-thioxo-1,3-thiazolidin-3-yl)hexanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-(methylamino)-2-phenylcyclohexan-1-one hydrochloride;
With
sodium hydroxide;
In
methanol;
at 20 ℃;
for 0.5h;
In
methanol; hexane; isopropyl alcohol;
Resolution of racemate;
- Guidance literature:
-
With
N,N,N,N,-tetramethylethylenediamine; nickel dichloride;
In
butan-1-ol;
at 130 ℃;
for 72h;
DOI:10.1016/S0957-4166(03)00433-6
- Guidance literature:
-
In
decalin;
at 190 ℃;
for 4h;
Microwave irradiation;
DOI:10.1039/c8nj03107j
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