TETRADECYL METHANE SULFATE

Base Information

• Chemical Name: TETRADECYL METHANE SULFATE
• CAS No.: 6222-16-8
• Molecular Formula: C15H32O3S
• Molecular Weight: 292.483
• Mol file: 6222-16-8.mol

Synonyms:1-Tetradecanol,methanesulfonate;1-methanesulfonyloxy-tetradecane;Tetradecanyl methanesulfonate;n-tetradecylmethanesulfonate;tetradecyl mesylate;mirystoylmethanesulfonate;methanesulfonic acid tetradecyl ester;

Chemical Property of TETRADECYL METHANE SULFATE

Chemical Property:

• Vapor Pressure: 3.09E-06mmHg at 25°C
• Boiling Point: 399.7°Cat760mmHg
• Flash Point: 195.5°C
• PSA: 51.75000
• Density: 0.963g/cm³
• LogP: 5.74450

Purity/Quality:

99% ^*data from raw suppliers

TETRADECYL METHANESULFONATE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRADECYL METHANE SULFATE

There total 3 articles about TETRADECYL METHANE SULFATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-Tetradecanol (112-72-1) + methanesulfonyl chloride (124-63-0) → tetradecyl mesylate (6222-16-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 0.666667h;

DOI:10.1002/ejoc.200300361

Reference yield: 95.0%

→ tetradecyl mesylate (6222-16-8)

Guidance literature:

Reference yield:

pentadecanoic acid methyl ester (7132-64-1) → tetradecyl mesylate (6222-16-8)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: pyridine / 24 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1080/14786419.2019.1686370

upstream raw materials:

1-Tetradecanol

methanesulfonyl chloride

pentadecanoic acid methyl ester

Downstream raw materials:

1-myristyl glycerol

3-[3-(2-Ethoxycarbonyl-ethyl)-4-tetradecyloxy-benzoyl]-benzoic acid ethyl ester

2-(tetradecylamino)ethan-1-ol

N,N-bis(2-hydroxyethyl)tetradecylamine

Refernces

• 1、 Coimbra, Elaine S.,De Almeida, Mauro V.,Junior, Celso O. R.,Taveira, Aline F.,Da Costa, Cristiane F.,De Almeida, Ana C.,Reis, Elaine F. C.,Da Silva, Adilson D.. "Synthesis and antileishmanial activity of lipidic amino alcohols". scheme or table. p. 233 - 235. Retrieved 2010/12/20.
• 2、 Pijper, Dirk,Bulten, Erna,Smisterova, Jarmila,Wagenaar, Anno,Hoekstra, Dick,Engberts, Jan B. F. N.,Hulst, Ron. "Novel Biodegradable Pyridinium Amphiphiles for Gene Delivery". . p. 4406 - 4412. Retrieved 2007/10/03.