Technology Process of Benzyl(dichloro)(chloromethyl)silane
There total 2 articles about Benzyl(dichloro)(chloromethyl)silane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzyl chloride;
With
magnesium;
In
diethyl ether;
at 20 ℃;
for 13h;
Inert atmosphere;
Schlenk technique;
(chloromethyl)trichlorosilane;
In
diethyl ether;
at 0 ℃;
for 14h;
Inert atmosphere;
Schlenk technique;
Reflux;
DOI:10.1002/anie.201813229
- Guidance literature:
-
Trichlor-chlormethyl-silan, Benzylmagnesiumchlorid;
- Guidance literature:
-
benzyl(chloromethyl)dichlorosilane;
With
lithium aluminium tetrahydride;
In
dibutyl ether;
at 0 - 20 ℃;
With
hydrogenchloride;
for 0.5h;
cooling;
DOI:10.1016/j.jorganchem.2007.01.035
