Cyclohex-2-en-1-amine;phosphoric acid

Base Information

• Chemical Name: Cyclohex-2-en-1-amine;phosphoric acid
• CAS No.: 90014-19-0
• Molecular Formula: C6H11N.H3O4P
• Molecular Weight: 195.155
• DSSTox Substance ID: DTXSID20522254
• Mol file: 90014-19-0.mol

Synonyms:90014-19-0;DTXSID20522254;Phosphoric acid--cyclohex-2-en-1-amine (1/1)

Chemical Property of Cyclohex-2-en-1-amine;phosphoric acid

Chemical Property:

• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 0
• Exact Mass: 195.06604493
• Heavy Atom Count: 12
• Complexity: 126

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC=CC(C1)N.OP(=O)(O)O

Technology Process of Cyclohex-2-en-1-amine;phosphoric acid

There total 2 articles about Cyclohex-2-en-1-amine;phosphoric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N,N-Bis(trimethylsilyl)-2-cyclohexen-1-ylamin (90014-17-8) → Hexamethyldisiloxane (107-46-0) + 2-Cyclohexen-1-ylamin-dihydrogenphosphat (90014-19-0)

Guidance literature:

With phosphoric acid;

Reference yield:

rac-3-bromocyclohexene (1521-51-3,113667-32-6) → 2-Cyclohexen-1-ylamin-dihydrogenphosphat (90014-19-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / hexamethyldisilazane / 8 h / Ambient temperature

2: 97 percent / 2 N H₃PO₄

With phosphoric acid; 1,1,1,3,3,3-hexamethyl-disilazane;

upstream raw materials:

N,N-Bis(trimethylsilyl)-2-cyclohexen-1-ylamin

rac-3-bromocyclohexene

Refernces