1-bromo-4-[(4-fluoro-3-nitrophenyl)sulfonyl]-2-nitrobenzene

Base Information

• Chemical Name: 1-bromo-4-[(4-fluoro-3-nitrophenyl)sulfonyl]-2-nitrobenzene
• CAS No.: 312-28-7
• Molecular Formula: C₁₂H₆BrFN₂O₆S
• Molecular Weight: 405.158
• Mol file: 312-28-7.mol

Synonyms:Sulfone,4-bromo-3-nitrophenyl 4-fluoro-3-nitrophenyl (8CI); NSC 18288

Chemical Property of 1-bromo-4-[(4-fluoro-3-nitrophenyl)sulfonyl]-2-nitrobenzene

Chemical Property:

• Vapor Pressure: 1E-10mmHg at 25°C
• Boiling Point: 528.5°Cat760mmHg
• Flash Point: 273.4°C
• Density: 1.826g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-bromo-4-[(4-fluoro-3-nitrophenyl)sulfonyl]-2-nitrobenzene

There total 3 articles about 1-bromo-4-[(4-fluoro-3-nitrophenyl)sulfonyl]-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-4-((4-fluorophenyl)sulfonyl)benzene (383-28-8) → (4-bromo-3-nitro-phenyl)-(4-fluoro-3-nitro-phenyl)-sulfone (312-28-7)

Guidance literature:

With sulfuric acid; nitric acid;

Reference yield:

bromobenzene (108-86-1,52753-63-6) → (4-bromo-3-nitro-phenyl)-(4-fluoro-3-nitro-phenyl)-sulfone (312-28-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride

2: sulfuric acid; nitric acid

With aluminium trichloride; sulfuric acid; nitric acid;

Reference yield:

4-Fluorobenzenesulfonyl chloride (349-88-2) → (4-bromo-3-nitro-phenyl)-(4-fluoro-3-nitro-phenyl)-sulfone (312-28-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride

2: sulfuric acid; nitric acid

With aluminium trichloride; sulfuric acid; nitric acid;

upstream raw materials:

1-bromo-4-((4-fluorophenyl)sulfonyl)benzene

bromobenzene

4-Fluorobenzenesulfonyl chloride