Benzamide, 2-(2-amino-2-oxoethoxy)-

Base Information

• Chemical Name: Benzamide, 2-(2-amino-2-oxoethoxy)-
• CAS No.: 90074-80-9
• Molecular Formula: C₉H₁₀N₂O₃
• Molecular Weight: 194.19
• Mol file: 90074-80-9.mol

Synonyms:2-Carbamoylmethoxy-benzoesaeure-amid;Salicylamid-O-acetamid;Salicylamid-O-essigsaeureamid;2-carbamoylmethoxy-benzoic acid amide;

Chemical Property of Benzamide, 2-(2-amino-2-oxoethoxy)-

Chemical Property:

• PSA: 97.39000
• LogP: 1.68350

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzamide, 2-(2-amino-2-oxoethoxy)-

There total 8 articles about Benzamide, 2-(2-amino-2-oxoethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-(2-ethoxy-2-oxoethoxy)benzoate (56424-77-2) → 2-carbamoylmethoxy-benzoic acid amide (90074-80-9)

Guidance literature:

With ammonia; at 100 ℃; im geschlossenen Rohr;

Reference yield:

2-azidocarbonylmethoxy-benzoic acid amide (108105-92-6) → 2-carbamoylmethoxy-benzoic acid amide (90074-80-9)

Guidance literature:

With ammonia;

DOI:10.1002/ardp.19552880809

Reference yield:

(2-Carbamoyl-phenoxy)-essigsaeure-methylester (90922-64-8) → 2-carbamoylmethoxy-benzoic acid amide (90074-80-9)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol; N₂H₄+H₂O

2: NaNO₂; aqueous HCl

3: ethanolic NH₃

With hydrogenchloride; methanol; ammonia; hydrazine hydrate; sodium nitrite;

DOI:10.1002/ardp.19552880809

upstream raw materials:

ethyl 2-(2-ethoxy-2-oxoethoxy)benzoate

2-azidocarbonylmethoxy-benzoic acid amide

salicylamide

Chloroacetamide

Refernces