Phosphonic acid, P-(2-methoxy-1-pyrrolidinyl)-, (1R,2S,5S)-5-methyl-2-(1-methylethyl)cyclohexyl phenyl ester

Base Information

• Chemical Name: Phosphonic acid, P-(2-methoxy-1-pyrrolidinyl)-, (1R,2S,5S)-5-methyl-2-(1-methylethyl)cyclohexyl phenyl ester
• CAS No.: 917615-83-9
• Molecular Formula: C21H34NO4P
• Molecular Weight: 395.479
• Mol file: 917615-83-9.mol

Synonyms:

Chemical Property of Phosphonic acid, P-(2-methoxy-1-pyrrolidinyl)-, (1R,2S,5S)-5-methyl-2-(1-methylethyl)cyclohexyl phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphonic acid, P-(2-methoxy-1-pyrrolidinyl)-, (1R,2S,5S)-5-methyl-2-(1-methylethyl)cyclohexyl phenyl ester

There total 1 articles about Phosphonic acid, P-(2-methoxy-1-pyrrolidinyl)-, (1R,2S,5S)-5-methyl-2-(1-methylethyl)cyclohexyl phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methanol (67-56-1) + C20H32NO3P (917615-71-5) → C21H34NO4P (917615-83-9)

Guidance literature:

With N,N,N,N-tetraethylammonium tetrafluoroborate; potassium hydrogencarbonate; at 20 ℃; Electrolysis;

DOI:10.1055/s-2006-950226

Reference yield: 84.0%

C21H34NO4P (917615-83-9) + allyl-trimethyl-silane (762-72-1) → menthyl phenyl(2-allylpyrrolidin-1-yl)phosphinate (917615-97-5)

Guidance literature:

C₂₁H₃₄NO₄P; With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 0.25h;

allyl-trimethyl-silane; In dichloromethane; at -78 - 20 ℃; Further stages.;

DOI:10.1055/s-2006-950226

upstream raw materials:

methanol

C₂₀H₃₂NO₃P

Downstream raw materials:

menthyl phenyl(2-allylpyrrolidin-1-yl)phosphinate

Refernces