Benzenamine, 4-(2,6-diphenyl-4-pyridinyl)-N,N-dimethyl-

Base Information

• Chemical Name: Benzenamine, 4-(2,6-diphenyl-4-pyridinyl)-N,N-dimethyl-
• CAS No.: 29312-59-2
• Molecular Formula: C25H22 N2
• Molecular Weight: 350.463
• Hs Code.: 2933399090
• European Community (EC) Number: 249-551-0
• DSSTox Substance ID: DTXSID7067453
• Nikkaji Number: J250.814A
• Wikidata: Q81994046
• Mol file: 29312-59-2.mol

Synonyms:29312-59-2;Benzenamine, 4-(2,6-diphenyl-4-pyridinyl)-N,N-dimethyl-;4-(2,6-Diphenyl-4-pyridyl)-N,N-dimethylaniline;EINECS 249-551-0;4-(2,6-diphenylpyridin-4-yl)-n,n-dimethylaniline;Oprea1_673984;SCHEMBL4353469;DTXSID7067453;C25H22N2;AKOS001031401;C25-H22-N2;NCGC00331431-01;AB01102994-03;2,6-diphenyl-4-(4'-dimethylaminophenyl)-pyridine;2,6-Diphenyl-4-[4-(dimethylamino)phenyl]pyridine;W-110752;4-(2,6-diphenylpyridin-4-yl)-N,N-dimethylbenzenamine;4-[p-(N,N-dimethylamino)phenyl]-2,6-diphenylpyridine;Z56800884

Chemical Property of Benzenamine, 4-(2,6-diphenyl-4-pyridinyl)-N,N-dimethyl-

Chemical Property:

• Vapor Pressure: 2.19E-10mmHg at 25°C
• Boiling Point: 506.6°Cat760mmHg
• Flash Point: 260.2°C
• PSA: 16.13000
• Density: 1.107g/cm³
• LogP: 6.14860
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 350.178298710
• Heavy Atom Count: 27
• Complexity: 402

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)C2=CC(=NC(=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Benzenamine, 4-(2,6-diphenyl-4-pyridinyl)-N,N-dimethyl-

There total 23 articles about Benzenamine, 4-(2,6-diphenyl-4-pyridinyl)-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

guanidine nitrate (113-00-8) + acetophenone (98-86-2) + 4-dimethylamino-chalcone (1030-27-9,22965-98-6,72758-79-3) → 4-(2,6-diphenylpyridin-4-yl)-N,N-dimethylaniline (29312-59-2)

Guidance literature:

for 0.0666667h; Microwave irradiation; neat (no solvent);

DOI:10.3184/174751912X13295721847185

Reference yield: 93.0%

4-dimethylamino-chalcone (1030-27-9,22965-98-6,72758-79-3) → 4-(2,6-diphenylpyridin-4-yl)-N,N-dimethylaniline (29312-59-2)

Guidance literature:

With guanidine hydrochloride; at 180 ℃; for 0.0833333h; Microwave irradiation; neat (no solvent);

DOI:10.1246/cl.2008.1048

Reference yield: 93.0%

4-(dimethylamino)chalcone (22965-98-6,72758-79-3,1030-27-9) → 4-(2,6-diphenylpyridin-4-yl)-N,N-dimethylaniline (29312-59-2)

Guidance literature:

With ammonium acetate; acetic acid; at 100 ℃; for 4h;

DOI:10.1016/j.tetlet.2006.01.162

upstream raw materials:

4-(4-dimethylamino-phenyl)-2,6-diphenyl-pyrylium; chloride

ammonium acetate

acetophenone

4-dimethylamino-benzaldehyde

Refernces

• 1、 Wang, De-Hui,Zhang, Yuan,Wang, Yu-Tong,Feng, Hui-Yan,Chen, Yong,Zhao, De-Zhi. "Silver(I) Complexes of Diphenylpyridines: Crystal Structures, Luminescence Studies, Theoretical Insights, and Biological Activities". . p. 323 - 332. Retrieved 2017/03/09.
• 2、 Alinezhad, Heshmatollah,Tajbakhsh, Mahmood,Ghobadi, Neda. "Nano-Fe3O4-supported, hydrogensulfate ionic liquid-catalyzed, one-pot synthesis of polysubstituted pyridines". supporting information. p. 1964 - 1976. Retrieved 2015/08/18.