16,17-Dihydro-17-isopropyl-15H-cyclopenta(a)phenanthrene

Base Information

• Chemical Name: 16,17-Dihydro-17-isopropyl-15H-cyclopenta(a)phenanthrene
• CAS No.: 5830-64-8
• Molecular Formula: C20H20
• Molecular Weight: 260.3728
• DSSTox Substance ID: DTXSID80973844
• Mol file: 5830-64-8.mol

Synonyms:16,17-Dihydro-17-isopropyl-15H-cyclopenta(a)phenanthrene;5830-64-8;15H-Cyclopenta(a)phenanthrene, 16,17-dihydro-17-isopropyl-;DTXSID80973844;17-(Propan-2-yl)gona-1(10),2,4,6,8,11,13-heptaene

Chemical Property of 16,17-Dihydro-17-isopropyl-15H-cyclopenta(a)phenanthrene

Chemical Property:

• Vapor Pressure: 5.36E-07mmHg at 25°C
• Boiling Point: 423.8°C at 760 mmHg
• Flash Point: 204.3°C
• Density: 1.09g/cm³
• XLogP3: 6.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 260.156500638
• Heavy Atom Count: 20
• Complexity: 344

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)C1CCC2=C1C=CC3=C2C=CC4=CC=CC=C43

Technology Process of 16,17-Dihydro-17-isopropyl-15H-cyclopenta(a)phenanthrene

There total 5 articles about 16,17-Dihydro-17-isopropyl-15H-cyclopenta(a)phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3'-Isopropyl-cyclopentenophenantren (5830-64-8)

Guidance literature:

With hydrogenchloride; amalgamated zinc;

DOI:10.1021/ja01249a031

Reference yield:

3H-Cyclopentaphenanthrene (219-08-9) → 3'-Isopropyl-cyclopentenophenantren (5830-64-8)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine

2: Pd-C / ethyl acetate / (hydrogenation)

With piperidine; palladium on activated charcoal; In ethyl acetate;

DOI:10.1039/j39660000963

Reference yield:

17-(Toluol-4-sulfonyloxy)-16,17-dihydro-15H-cyclopentaphenanthren (5837-15-0) → 3'-Isopropyl-cyclopentenophenantren (5830-64-8)

Guidance literature:

Multi-step reaction with 3 steps

1: collidine / (heating)

2: piperidine

3: Pd-C / ethyl acetate / (hydrogenation)

With piperidine; 2,3,5-trimethyl-pyridine; palladium on activated charcoal; In ethyl acetate;

DOI:10.1039/j39660000963

upstream raw materials:

17-Isopropyliden-cyclopentaphenanthren

3H-Cyclopentaphenanthrene

17-(Toluol-4-sulfonyloxy)-16,17-dihydro-15H-cyclopentaphenanthren